Miniaturization of an extraction protocol for the monitoring of pesticides and polar transformation products in biotic matrices.

Animals Chromatography, Liquid Miniaturization Pesticide Residues / analysis Pesticides / analysis Solid Phase Extraction Tandem Mass Spectrometry
Fish LC-MS/MS Macroinvertebrate Miniaturization Polar pesticide Transformation product

Journal

Chemosphere
ISSN: 1879-1298
Titre abrégé: Chemosphere
Pays: England
ID NLM: 0320657

Informations de publication

Date de publication:
Dec 2021
Historique:
received: 03 05 2021
revised: 16 06 2021
accepted: 17 06 2021
pubmed: 2 7 2021
medline: 5 10 2021
entrez: 1 7 2021
Statut: ppublish

Résumé

Monitoring pesticides in the environment requires the use of sensitive analytical methods. However, existing methods are generally not suitable for analyzing small organisms, as they require large matrix masses. This study explores the development of a miniaturized extraction protocol for the monitoring of small organisms, based on only 30 mg of matrix. The miniaturized sample preparation was developed using fish and macroinvertebrate matrices. It allowed the characterization of 41 pesticides and transformation products (log P from -1.9 to 4.8) in small samples with LC-MS/MS, based on European guidelines (European Commission DG-SANTE, 2019). Quantification limits ranged from 3 to 460 ng g

Identifiants

DOI: 10.1016/j.chemosphere.2021.131292 PMID: 34198062
pubmed: 34198062
pii: S0045-6535(21)01764-1
doi: 10.1016/j.chemosphere.2021.131292
pii:
doi:

Substances chimiques

Pesticide Residues 0
Pesticides 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

131292

Informations de copyright

Copyright © 2021 Elsevier Ltd. All rights reserved.

Auteurs

Vincent Dufour (V)

Université de Lorraine, INRAE, URAFPA, F-54000, Nancy, France; Univ Lyon, CNRS, Université Claude Bernard Lyon 1, Institut des Sciences Analytiques, UMR 5280, 5 rue de la Doua, F-69100, Villeurbanne, France. Electronic address: vincent.dufour@univ-lorraine.fr.

Laure Wiest (L)

Univ Lyon, CNRS, Université Claude Bernard Lyon 1, Institut des Sciences Analytiques, UMR 5280, 5 rue de la Doua, F-69100, Villeurbanne, France.

Sylvain Slaby (S)

Université de Lorraine, INRAE, URAFPA, F-54000, Nancy, France.

François Le Cor (F)

Université de Lorraine, INRAE, URAFPA, F-54000, Nancy, France; LHN, Laboratoire d'Hydrologie de Nancy, ANSES, 40 rue Lionnois, F-54000, Nancy, France.

Lucile Auger (L)

Université de Lorraine, INRAE, URAFPA, F-54000, Nancy, France; Office Français de la Biodiversité, Montfort, F-01330, Birieux, France.

Olivier Cardoso (O)

Office Français de la Biodiversité, 9 Avenue Buffon, F-45071, Orléans, France.

Laurence Curtet (L)

Office Français de la Biodiversité, Montfort, F-01330, Birieux, France.

Laure Pasquini (L)

LHN, Laboratoire d'Hydrologie de Nancy, ANSES, 40 rue Lionnois, F-54000, Nancy, France.

Xavier Dauchy (X)

LHN, Laboratoire d'Hydrologie de Nancy, ANSES, 40 rue Lionnois, F-54000, Nancy, France.

Emmanuelle Vulliet (E)

Univ Lyon, CNRS, Université Claude Bernard Lyon 1, Institut des Sciences Analytiques, UMR 5280, 5 rue de la Doua, F-69100, Villeurbanne, France.

Damien Banas (D)

Université de Lorraine, INRAE, URAFPA, F-54000, Nancy, France. Electronic address: damien.banas@univ-lorraine.fr.

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Classifications MeSH

questionsmedicales.fr › Eucaryotes › Animaux › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Technologie, industrie et agriculture › Technologie › Miniaturisation › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Pollution de l'environnement › Charge corporelle › Résidus de pesticides › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Actions chimiques et utilisations › Actions toxiques › Pesticides › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Fractionnement chimique › Extraction en phase solide › Miniaturization of an extraction protocol for...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Miniaturization of an extraction protocol for...