High Resolution Patterning of an Organic-Inorganic Photoresin for the Fabrication of Platinum Microstructures.

direct lithography metal printing nanofabrication platinum microstructures printed electronics two-photon lithography

Journal

Advanced materials (Deerfield Beach, Fla.)
ISSN: 1521-4095
Titre abrégé: Adv Mater
Pays: Germany
ID NLM: 9885358

Informations de publication

Date de publication:
Sep 2021
Historique:
revised: 09 06 2021
received: 12 03 2021
pubmed: 3 8 2021
medline: 3 8 2021
entrez: 2 8 2021
Statut: ppublish

Résumé

Platinum (Pt) is an interesting material for many applications due to its high chemical resilience, outstanding catalytic activity, high electrical conductivity, and high melting point. However, microstructuring and especially 3D microstructuring of platinum is a complex process, based on expensive and specialized equipment often suffering from very slow processing speeds. In this work, organic-inorganic photoresins, which can be structured using direct optical lithography as well as two-photon lithography (TPL) with submicrometer resolution and high-throughput is presented. The printed structures are subsequently converted to high-purity platinum using thermal debinding of the binder and reduction of the salt. With this technique, complex 3D structures with a 3D resolution of 300 nm were fabricated. At a layer thickness of 35 nm, the patterns reach a high conductivity of 67% compared to bulk platinum. Microheaters, thermocouple sensors as well as a Lab-on-a-Chip system are presented as exemplary applications. This technology will enable a broad range of application from electronics, sensing and heating elements to 3D photonics and metamaterials.

Identifiants

pubmed: 34337801
doi: 10.1002/adma.202101992
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e2101992

Subventions

Organisme : German Ministry of Education and Research
ID : 03X5527
Organisme : European Union's Horizon 2020 research and innovation programme
ID : 816006
Organisme : Deutsche Forschungsgemeinschaft
Organisme : Germany's Excellence Strategy
ID : EXC-2193/1 - 390951807
Organisme : Research Cluster "Interactive and Programmable Materials
Organisme : Carl Zeiss Foundation
Organisme : European Research Council
Pays : International

Informations de copyright

© 2021 The Authors. Advanced Materials published by Wiley-VCH GmbH.

Références

CRC Handbook of Chemistry and Physics: A Ready-Reference Book of Chemical and Physical Data, CRC Press, Boca Raton, FL 2017.
J. C. Chaston, Platinum Met. Rev. 1982, 26, 7.
C.-H. Wu, D. Kang, P.-H. Chen, Y.-C. Tai, Sens. Actuators, A 2016, 241, 135.
F. Ejeian, S. Azadi, A. Razmjou, Y. Orooji, A. Kottapalli, M. E. Warkiani, M. Asadnia, Sens. Actuators, A 2019, 295, 483.
M. Odijk, A. Baumann, W. Lohmann, F. T. G. van den Brink, W. Olthuis, U. Karst, A. van den Berg, Lab Chip 2009, 9, 1687.
M. Cosetti, J. T. Roland, Oper. Tech. Otolaryngology-Head and Neck Surgery 2010, 21, 223.
A. Kloke, F. von Stetten, R. Zengerle, S. Kerzenmacher, Adv. Mater. 2011, 23, 4976.
Y. Zhu, B. Chen, M. Qin, J. Huang, Q. Huang, J. Micromech. Microeng. 2015, 25, 085011.
W. Sripumkhai, A. Lekwichai, W. Bunjongpru, S. Porntheeraphat, B. Tunhoo, E. Ratanaudomphisut, T. Kamsri, C. Hruanun, A. Poyai, J. Nukeaw, Adv. Mater. Res. 2010, 93-94, 129.
F. Samaeifar, H. Hajghassem, A. Afifi, H. Abdollahi, Sens. Rev. 2015, 35, 116.
S. Youssef, J. Podlecki, R. Al Asmar, B. Sorli, O. Cyril, A. Foucaran, J. Microelectromech. Syst. 2009, 18, 414.
A. I. K. Lao, T. M. H. Lee, I.-M. Hsing, N. Y. Ip, Sens. Actuators, A 2000, 84, 11.
T.-H. Chang, D. Struk, M. Navaei, V. M. Doroshenko, V. Laiko, E. Moskovets, K. Novoselov, J.-M. D. Dimandja, P. J. Hesketh, Sens. Actuators, B 2020, 307, 127588.
F. Shaun, S. Sarkar, F. Marty, P. Poulichet, W. Cesar, E. Nefzaoui, T. Bourouina, J. Micromech. Microeng. 2018, 28, 074002.
M. Yang, F. Qu, Y. Lu, Y. He, G. Shen, R. Yu, Biomaterials 2006, 27, 5944.
J. H. Yuan, K. Wang, X. H. Xia, Adv. Funct. Mater. 2005, 15, 803.
W. E. Mustain, H. Kim, S. Prakash, J. Stark, T. Osborn, P. A. Kohl, Electrochem. Solid-State Lett. 2007, 10, B210.
H.-F. Wang, Z.-P. Liu, J. Am. Chem. Soc. 2008, 130, 10996.
B. O'Regan, M. Grätzel, Nature 1991, 353, 737.
L. Chen, W. Tan, J. Zhang, X. Zhou, X. Zhang, Y. Lin, Electrochim. Acta 2010, 55, 3721.
M. Özkan, S. G. Hashmi, J. Halme, A. Karakoç, T. Sarikka, J. Paltakari, P. D. Lund, Org. Electron. 2017, 44, 159.
D. J. Frankel, S. C. Moulzolf, M. P. da Cunha, R. J. Lad, Surf. Coat. Technol. 2015, 284, 215.
R. Zhong, X. Pan, L. Jiang, Z. Dai, J. Qin, B. Lin, Electrophoresis 2009, 30, 1297.
J. El-Ali, I. R. Perch-Nielsen, C. R. Poulsen, D. D. Bang, P. Telleman, A. Wolff, Sens. Actuators, A 2004, 110, 3.
S. Shukla, D. Stanier, M. S. Saha, J. Stumper, M. Secanell, J. Electrochem. Soc. 2016, 163, F677.
G. Cummins, M. P. Y. Desmulliez, Circuit World 2012, 38, 193.
M. Zea, A. Moya, M. Fritsch, E. Ramon, R. Villa, G. Gabriel, ACS Appl. Mater. Interfaces 2019, 11, 15160.
P. Yang, L. Zhang, D. J. Kang, R. Strahl, T. Kraus, Adv. Opt. Mater. 2020, 8, 1901429.
A. Waldbaur, H. Rapp, K. Länge, B. E. Rapp, Anal. Methods 2011, 3, 2681.
Y.-G. Park, H. Min, H. Kim, A. Zhexembekova, C. Y. Lee, J.-U. Park, Nano Lett. 2019, 19, 4866.
M. Manoccio, M. Esposito, A. Passaseo, M. Cuscunà, V. Tasco, Micromachines 2021, 12, 6.
C. Shemelya, D. DeMeo, N. P. Latham, X. Wu, C. Bingham, W. Padilla, T. E. Vandervelde, Appl. Phys. Lett. 2014, 104, 201113.
J. Kaschke, M. Wegener, Nanophotonics 2016, 5, 510.
J. Luo, R. Pohl, L. Qi, G.-W. Römer, C. Sun, D. Lohse, C. W. Visser, Small 2017, 13, 1602553.
M. Zenou, A. Sa'ar, Z. Kotler, Sci. Rep. 2015, 5, 17265.
J. Hu, M.-F. Yu, Science 2010, 329, 313.
A. P. Suryavanshi, M.-F. Yu, Nanotechnology 2007, 18, 105305.
V. Tasco, M. Esposito, F. Todisco, A. Benedetti, M. Cuscunà, D. Sanvitto, A. Passaseo, Appl. Phys. A 2016, 122, 280.
J. D. Fowlkes, R. Winkler, B. B. Lewis, M. G. Stanford, H. Plank, P. D. Rack, ACS Nano 2016, 10, 6163.
A. Botman, J. J. L. Mulders, C. W. Hagen, Nanotechnology 2009, 20, 372001.
S. Maruo, O. Nakamura, S. Kawata, Opt. Lett. 1997, 22, 132.
V. Hahn, P. Kiefer, T. Frenzel, J. Qu, E. Blasco, C. Barner-Kowollik, M. Wegener, Adv. Funct. Mater. 2020, 30, 1907795.
B. W. Pearre, C. Michas, J.-M. Tsang, T. J. Gardner, T. M. Otchy, Addit. Manuf. 2019, 30, 100887.
A. Vyatskikh, S. Delalande, A. Kudo, X. Zhang, C. M. Portela, J. R. Greer, Nat. Commun. 2018, 9, 593.
D. W. Yee, M. L. Lifson, B. W. Edwards, J. R. Greer, Adv. Mater. 2019, 31, 1901345.
X. Zhang, H. Xie, M. Fujii, H. Ago, K. Takahashi, T. Ikuta, H. Abe, T. Shimizu, Appl. Phys. Lett. 2005, 86, 171912.
C. Sun, X. Zhang, Sens. Actuators, A 2002, 101, 364.
E. Wiberg, N. Wiberg, Lehrbuch der anorganischen Chemie, Walter De Gruyter, Berlin 2007.
M. U. Kopp, A. J. de Mello, A. Manz, Science 1998, 280, 1046.
D. Moschou, N. Vourdas, G. Kokkoris, G. Papadakis, J. Parthenios, S. Chatzandroulis, A. Tserepi, Sens. Actuators, B 2014, 199, 470.
M. J. Jebrail, A. H. C. Ng, V. Rai, R. Hili, A. K. Yudin, A. R. Wheeler, Angew. Chem., Int. Ed. 2010, 49, 8625.
N. Vergauwe, D. Witters, F. Ceyssens, S. Vermeir, B. Verbruggen, R. Puers, J. Lammertyn, J. Micromech. Microeng. 2011, 21, 054026.
R. S. Sista, A. E. Eckhardt, V. Srinivasan, M. G. Pollack, S. Palanki, V. K. Pamula, Lab Chip 2008, 8, 2188.
A. Waldbaur, B. Waterkotte, K. Schmitz, B. E. Rapp, Small 2012, 8, 1570.
A. Botman, J. J. L. Mulders, R. Weemaes, S. Mentink, Nanotechnology 2006, 17, 3779.
E. U. Donev, J. T. Hastings, Nano Lett. 2009, 9, 2715.
M. Lunzer, L. Shi, O. G. Andriotis, P. Gruber, M. Markovic, P. J. Thurner, D. Ossipov, R. Liska, A. Ovsianikov, Angew. Chem., Int. Ed. 2018, 57, 15122.
R. Paschotta, Field Guide to Lasers, Vol. FG12, SPIE, Bellingham, WA 2008, p. 152.

Auteurs

Manuel Luitz (M)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.

Markus Lunzer (M)

UpNano GmbH, Modecenterstraße 22/D6, Vienna, 1030, Austria.

Andreas Goralczyk (A)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.

Markus Mader (M)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.

Sagar Bhagwat (S)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.

Andreas Warmbold (A)

Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Straße 21, 79104, Freiburg, Germany.

Dorothea Helmer (D)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.
Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Straße 21, 79104, Freiburg, Germany.
FIT Freiburg Center of Interactive Materials and Bioinspired Technologies, University of Freiburg, Georges-Köhler-Allee 105, 79110, Freiburg, Germany.

Frederik Kotz (F)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.
Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Straße 21, 79104, Freiburg, Germany.

Bastian E Rapp (BE)

Laboratory of Process Technology, NeptunLab, Department of Microsystems Engineering (IMTEK) University of Freiburg, Georges-Köhler-Allee 103, 79110, Freiburg, Germany.
Freiburg Materials Research Center (FMF), University of Freiburg, Stefan-Meier-Straße 21, 79104, Freiburg, Germany.
FIT Freiburg Center of Interactive Materials and Bioinspired Technologies, University of Freiburg, Georges-Köhler-Allee 105, 79110, Freiburg, Germany.

Classifications MeSH