A practical approach for gmp-compliant validation of real-time PCR method for mycoplasma detection in human mesenchymal stromal cells as advanced therapy medicinal product.


Journal

Biologicals : journal of the International Association of Biological Standardization
ISSN: 1095-8320
Titre abrégé: Biologicals
Pays: England
ID NLM: 9004494

Informations de publication

Date de publication:
Sep 2021
Historique:
received: 28 09 2020
revised: 26 07 2021
accepted: 30 07 2021
pubmed: 8 8 2021
medline: 24 11 2021
entrez: 7 8 2021
Statut: ppublish

Résumé

Manufacturing of human Mesenchymal Stromal Cells as advanced therapy medicinal product (ATMP) for clinical use involves an ex vivo expansion, which leads to a risk of contamination by microbiological agents. Even if manufacturing under Good Manufacturing Practice (GMP) license minimizes this risk, contamination of cell cultures by mycoplasmas still represents a widespread problem. Furthermore, the absence of mycoplasma contamination represents one of ATMPs release criteria. Since July 2007, European Pharmacopoeia (EuPh) offers the possibility to replace official mycoplasma detection methods with Nucleic Acid Amplification techniques, after suitable validation. As an Italian authorized Cell Factory, we developed an in-house GMP-compliant validation of real-time PCR method for mycoplasma detection in human Mesenchymal Stromal Cells, according to EuPh sec. 2.6.7 and International Conference on Harmonization Q The study was performed in compliance with GMP international requirements with MycoSEQ™ Mycoplasma Detection Assay (Thermofisher) on QuantStudio5 real-Time PCR (Applied Biosystems). Assay validation was developed to evaluate sensitivity, interferences matrix-related, specificity and robustness. MycoSEQ™ Mycoplasma Detection Assay has been successfully validated on human Mesenchymal Stromal Cells as results comply with validation protocol acceptance criteria. MycoSEQ™ Mycoplasma Detection Assay is a fast, sensitive and specific PCR-based Nucleic Acid Test assay that can be used as an alternative to official mycoplasma test methods for lot release of human Mesenchymal Stromal Cells as advanced therapy medicinal product (ATMP). Moreover, our study underlines the presence of interference on real-time PCR reaction due to matrix composition, pointing out a practical approach for method validation (i.e interference removal).

Sections du résumé

BACKGROUND BACKGROUND
Manufacturing of human Mesenchymal Stromal Cells as advanced therapy medicinal product (ATMP) for clinical use involves an ex vivo expansion, which leads to a risk of contamination by microbiological agents. Even if manufacturing under Good Manufacturing Practice (GMP) license minimizes this risk, contamination of cell cultures by mycoplasmas still represents a widespread problem. Furthermore, the absence of mycoplasma contamination represents one of ATMPs release criteria. Since July 2007, European Pharmacopoeia (EuPh) offers the possibility to replace official mycoplasma detection methods with Nucleic Acid Amplification techniques, after suitable validation. As an Italian authorized Cell Factory, we developed an in-house GMP-compliant validation of real-time PCR method for mycoplasma detection in human Mesenchymal Stromal Cells, according to EuPh sec. 2.6.7 and International Conference on Harmonization Q
MATERIALS AND METHODS METHODS
The study was performed in compliance with GMP international requirements with MycoSEQ™ Mycoplasma Detection Assay (Thermofisher) on QuantStudio5 real-Time PCR (Applied Biosystems). Assay validation was developed to evaluate sensitivity, interferences matrix-related, specificity and robustness.
RESULTS RESULTS
MycoSEQ™ Mycoplasma Detection Assay has been successfully validated on human Mesenchymal Stromal Cells as results comply with validation protocol acceptance criteria.
CONCLUSIONS CONCLUSIONS
MycoSEQ™ Mycoplasma Detection Assay is a fast, sensitive and specific PCR-based Nucleic Acid Test assay that can be used as an alternative to official mycoplasma test methods for lot release of human Mesenchymal Stromal Cells as advanced therapy medicinal product (ATMP). Moreover, our study underlines the presence of interference on real-time PCR reaction due to matrix composition, pointing out a practical approach for method validation (i.e interference removal).

Identifiants

pubmed: 34362616
pii: S1045-1056(21)00070-1
doi: 10.1016/j.biologicals.2021.07.006
pii:
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

31-40

Informations de copyright

Copyright © 2021 International Alliance for Biological Standardization. Published by Elsevier Ltd. All rights reserved.

Auteurs

V Becherucci (V)

Quality Control Laboratory, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy. Electronic address: valentina.becherucci@meyer.it.

L Curini (L)

Quality Control Laboratory, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

R Ceccantini (R)

Quality Control Laboratory, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

S Bisin (S)

Production Unit, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

V Gori (V)

Production Unit, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

F Gentile (F)

Quality Control Laboratory, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

E De Rienzo (E)

Production Unit, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

L Piccini (L)

Production Unit, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

B Bindi (B)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

P Pavan (P)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

V Cunial (V)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

E Allegro (E)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

S Ermini (S)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

F Brugnolo (F)

Immunohematology and Transfusion Medicine, "A. Meyer" University Children's Hospital, Florence, Italy.

F Bambi (F)

Quality Control Laboratory, Cell Factory Meyer, "A. Meyer" University Children's Hospital, Florence, Italy.

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Classifications MeSH