Novel Non-Congeneric Derivatives of the Choline Kinase Alpha Inhibitor ICL-CCIC-0019.

ICL-CCIC-0019 PIK4CB PSMA choline kinase alpha (CHKA) inhibitor prodrug targeted drug delivery

Journal

Pharmaceutics
ISSN: 1999-4923
Titre abrégé: Pharmaceutics
Pays: Switzerland
ID NLM: 101534003

Informations de publication

Date de publication:
14 Jul 2021
Historique:
received: 22 06 2021
revised: 06 07 2021
accepted: 09 07 2021
entrez: 10 8 2021
pubmed: 11 8 2021
medline: 11 8 2021
Statut: epublish

Résumé

Choline kinase alpha (CHKA) is a promising target for the development of cancer therapeutics. We have previously reported ICL-CCIC-0019, a potent CHKA inhibitor with high cellular activity but with some unfavorable pharmacological properties. In this work, we present an active analogue of ICL-CCIC-0019 bearing a piperazine handle (CK146) to facilitate further structural elaboration of the pharmacophore and thus improve the biological profile. Two different strategies were evaluated in this study: (1) a prodrug approach whereby selective CHKA inhibition could be achieved through modulating the activity of CK146, via the incorporation of an ε-(Ac) Lys motif, cleavable by elevated levels of histone deacetylase (HDAC) and cathepsin L (CTSL) in tumour cells; (2) a prostate-specific membrane antigen (PSMA) receptor targeted delivery strategy. Prodrug (CK145) and PSMA-targeted (CK147) derivatives were successfully synthesized and evaluated in vitro. While the exploitation of CK146 in those two strategies did not deliver the expected results, important and informative structure-activity relationships were observed and have been reported.

Identifiants

pubmed: 34371769
pii: pharmaceutics13071078
doi: 10.3390/pharmaceutics13071078
pmc: PMC8309005
pii:
doi:

Types de publication

Journal Article

Langues

eng

Subventions

Organisme : China Sponsorship Council
ID : N/A
Organisme : Medical Research Council
ID : MR/M015858/1
Pays : United Kingdom
Organisme : NIHR Imperial Biomedical Research Centre
ID : WSCC_P62585
Organisme : Imperial Experimental Cancer Medicine Centre
ID : C1312/A25149
Organisme : National Cancer Imaging Translational Accelerator
ID : C2536/A28680

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Auteurs

Ning Wang (N)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Diana Brickute (D)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Marta Braga (M)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Chris Barnes (C)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Haonan Lu (H)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Louis Allott (L)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.
Positron Emission Tomography Research Centre, Faculty of Health Sciences, University of Hull, Kingston upon Hull HU6 7RX, UK.

Eric O Aboagye (EO)

Comprehensive Cancer Imaging Centre, Department of Surgery and Cancer, Faculty of Medicine, Imperial College London, Hammersmith Hospital, London W12 0NN, UK.

Classifications MeSH