Synthesis and evaluation of squaramide and thiosquaramide inhibitors of the DNA repair enzyme SNM1A.


Journal

Bioorganic & medicinal chemistry
ISSN: 1464-3391
Titre abrégé: Bioorg Med Chem
Pays: England
ID NLM: 9413298

Informations de publication

Date de publication:
15 09 2021
Historique:
received: 03 06 2021
revised: 05 08 2021
accepted: 07 08 2021
pubmed: 6 9 2021
medline: 31 12 2021
entrez: 5 9 2021
Statut: ppublish

Résumé

SNM1A is a zinc-dependent nuclease involved in the removal of interstrand crosslink lesions from DNA. Inhibition of interstrand crosslink repair enzymes such as SNM1A is a promising strategy for improving the efficacy of crosslinking chemotherapy drugs. Initial studies have demonstrated the feasibility of developing SNM1A inhibitors, but the full potential of this enzyme as a drug target has yet to be explored. Herein, the synthesis of a family of squaramide- and thiosquaramide-bearing nucleoside derivatives and their evaluation as SNM1A inhibitors is reported. A gel electrophoresis assay was used to identify nucleoside derivatives bearing an N-hydroxysquaramide or squaric acid moiety at the 3'-position, and a thymidine derivative bearing a 5'-thiosquaramide, as candidate SNM1A inhibitors. Quantitative IC

Identifiants

pubmed: 34482229
pii: S0968-0896(21)00377-1
doi: 10.1016/j.bmc.2021.116369
pmc: PMC8607331
pii:
doi:

Substances chimiques

Enzyme Inhibitors 0
squaramide 0
Quinine A7V27PHC7A
DNA Repair Enzymes EC 6.5.1.-

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

116369

Informations de copyright

Copyright © 2021 The Authors. Published by Elsevier Ltd.. All rights reserved.

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Auteurs

Mark Berney (M)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland.

William Doherty (W)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland.

Werner Theodor Jauslin (WT)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland.

Manav T Manoj (M)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland.

Eva-Maria Dürr (EM)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland.

Joanna Francelle McGouran (JF)

School of Chemistry & Trinity Biomedical Sciences Institute, Trinity College Dublin, The University of Dublin, Ireland. Electronic address: jmcgoura@tcd.ie.

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Classifications MeSH