Determination of nickel in daphne tea extract and lake water samples by flame atomic absorption spectrophotometry with a zirconium-coated T-shaped slotted quartz tube-atom trap and photochemical vapor generation sample introduction.
Atomic absorption spectrometry
Daphne tea
Nickel
Photochemical vapor generation
Quartz tube-atom trap
Journal
Environmental monitoring and assessment
ISSN: 1573-2959
Titre abrégé: Environ Monit Assess
Pays: Netherlands
ID NLM: 8508350
Informations de publication
Date de publication:
06 Sep 2021
06 Sep 2021
Historique:
received:
24
04
2021
accepted:
27
08
2021
entrez:
6
9
2021
pubmed:
7
9
2021
medline:
9
9
2021
Statut:
epublish
Résumé
Nickel determination is important because of its use in many industrial areas and its negative effects on human health. In this study, an ultraviolet-based photochemical vapor generation (UV-PVG) setup was combined with a T-shaped zirconium-coated slotted quartz tube-atom trapping (T-SQT-AT) apparatus to boost the sensitivity of a flame atomic absorption spectrophotometer for nickel determination. Nickel was separated from the sample matrix by converting it into its volatile species prior to online preconcentration by trapping on the zirconium-coated T-SQT inner surface. Analytical performance was maximized by optimizing all variable conditions. The limit of detection (LOD) and limit of quantification (LOQ) were found as 10 and 33 µg/L, respectively. Daphne tea and lake water samples were analyzed under optimum conditions, and there was no detectable nickel in the samples. For this purpose, spiking experiments were carried out for the samples in order to evaluate the applicability and accuracy of the method. The percent recovery values calculated for the two samples spiked at three different concentrations ranged between 90 and 112%. To our best knowledge, this is the first study in literature where UV-PVG was combined with T-SQT-AT for the determination of nickel in daphne tea and lake water samples prior to FAAS determination.
Identifiants
pubmed: 34487242
doi: 10.1007/s10661-021-09430-2
pii: 10.1007/s10661-021-09430-2
doi:
Substances chimiques
Plant Extracts
0
Tea
0
Water
059QF0KO0R
Quartz
14808-60-7
Nickel
7OV03QG267
Zirconium
C6V6S92N3C
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
627Subventions
Organisme : Türkiye Bilimsel ve Teknolojik Araştirma Kurumu
ID : 117Z380
Informations de copyright
© 2021. The Author(s), under exclusive licence to Springer Nature Switzerland AG.
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