Thiol Functionalised Supports for Controlled Metal Nanoparticle Formation for Improved C-C Coupling.
CC coupling
catalysis
nanoparticles
palladium
supported catalysts
Journal
Chemistry, an Asian journal
ISSN: 1861-471X
Titre abrégé: Chem Asian J
Pays: Germany
ID NLM: 101294643
Informations de publication
Date de publication:
15 Nov 2021
15 Nov 2021
Historique:
revised:
08
09
2021
received:
30
06
2021
pubmed:
11
9
2021
medline:
11
9
2021
entrez:
10
9
2021
Statut:
ppublish
Résumé
The myriad applications of metal nanoparticle systems have individual demands on their size, shape and electronic states, demanding novel synthetic methods to optimise these properties. Herein we report our method of exploiting strong thiol-Pd binding as a precursor for forming small, uniform Pd nanoparticles on activation. We validate our approach with a range of characterisation techniques and contrast our design strategy with an analogous wetness impregnation method, showing the drastic improvements for catalytic C-C coupling. The presence of the thiol groups offers greater control over nanoparticle formation, particularly temperature resolution on activation, potentially allowing more targeted nanoparticle formation procedures.
Identifiants
pubmed: 34506678
doi: 10.1002/asia.202100732
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
3610-3614Subventions
Organisme : TotalEnergies "Consortium on Metal Nanocatalysis" project
Organisme : AdvanSix
Organisme : Honeywell LLC
Informations de copyright
© 2021 Wiley-VCH GmbH.
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