In Situ Formation of Nano Ni-Co Oxyhydroxide Enables Water Oxidation Electrocatalysts Durable at High Current Densities.
CO
2 reduction
PGM-free X-ray absorption spectroscopy
cryomilling
oxygen evolution reaction
Journal
Advanced materials (Deerfield Beach, Fla.)
ISSN: 1521-4095
Titre abrégé: Adv Mater
Pays: Germany
ID NLM: 9885358
Informations de publication
Date de publication:
Nov 2021
Nov 2021
Historique:
revised:
04
08
2021
received:
19
05
2021
pubmed:
21
9
2021
medline:
21
9
2021
entrez:
20
9
2021
Statut:
ppublish
Résumé
The oxygen evolution reaction (OER) limits the energy efficiency of electrocatalytic systems due to the high overpotential symptomatic of poor reaction kinetics; this problem worsens over time if the performance of the OER electrocatalyst diminishes during operation. Here, a novel synthesis of nanocrystalline Ni-Co-Se using ball milling at cryogenic temperature is reported. It is discovered that, by anodizing the Ni-Co-Se structure during OER, Se ions leach out of the original structure, allowing water molecules to hydrate Ni and Co defective sites, and the nanoparticles to evolve into an active Ni-Co oxyhydroxide. This transformation is observed using operando X-ray absorption spectroscopy, with the findings confirmed using density functional theory calculations. The resulting electrocatalyst exhibits an overpotential of 279 mV at 0.5 A cm
Identifiants
pubmed: 34541731
doi: 10.1002/adma.202103812
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e2103812Subventions
Organisme : Natural Sciences and Engineering Research Council (NSERC) of Canada
Organisme : Vanier Canada Graduate Scholarship
Organisme : Canadian Centre for Electron Microscopy
Organisme : Advanced Photon Source, an Office of Science User Facility
Organisme : U.S. Department of Energy (DOE) Office of Science
Organisme : Argonne National Laboratory
ID : DE-AC02-06CH11357
Organisme : Engineered Nickel Catalysts for Electrochemical Clean Energy
ID : RGPNM 477963-2015
Organisme : Natural Sciences and Engineering Research Council of Canada
Informations de copyright
© 2021 Wiley-VCH GmbH.
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