Solvent-Switched Manganese(I)-Catalyzed Regiodivergent Distal vs Proximal C-H Alkylation of Imidazopyridine with Maleimide.


Journal

Organic letters
ISSN: 1523-7052
Titre abrégé: Org Lett
Pays: United States
ID NLM: 100890393

Informations de publication

Date de publication:
01 10 2021
Historique:
pubmed: 21 9 2021
medline: 21 9 2021
entrez: 20 9 2021
Statut: ppublish

Résumé

A sustainable Mn(I)-catalyzed exclusive solvent-dependent functionalization of imidazopyridine with maleimide via an electrophilic metalation at the distal (in 2,2,2-trifluoroethanol (TFE)) and chelation assisted at the proximal (in tetrahydrofuran (THF)) has been developed. The strategy was successfully applied to the drug Zolimidine and a broad range of substrates, thereby reflecting the method's versatility.

Identifiants

pubmed: 34543041
doi: 10.1021/acs.orglett.1c02536
doi:

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

7370-7375

Auteurs

Subhendu Ghosh (S)

Department of Chemistry, Indian Institute of Technology Guwahati, North Guwahati 781039, India.

Tamanna Khandelia (T)

Department of Chemistry, Indian Institute of Technology Guwahati, North Guwahati 781039, India.

Bhisma K Patel (BK)

Department of Chemistry, Indian Institute of Technology Guwahati, North Guwahati 781039, India.

Classifications MeSH