Pink-beam serial femtosecond crystallography for accurate structure-factor determination at an X-ray free-electron laser.
XFELs
data-quality indicators
de novo protein structure determination
large bandwidths
pink beams
serial femtosecond crystallography
single-wavelength anomalous diffraction
Journal
IUCrJ
ISSN: 2052-2525
Titre abrégé: IUCrJ
Pays: England
ID NLM: 101623101
Informations de publication
Date de publication:
01 Nov 2021
01 Nov 2021
Historique:
received:
01
06
2021
accepted:
05
08
2021
entrez:
22
11
2021
pubmed:
23
11
2021
medline:
23
11
2021
Statut:
epublish
Résumé
Serial femtosecond crystallography (SFX) at X-ray free-electron lasers (XFELs) enables essentially radiation-damage-free macromolecular structure determination using microcrystals that are too small for synchrotron studies. However, SFX experiments often require large amounts of sample in order to collect highly redundant data where some of the many stochastic errors can be averaged out to determine accurate structure-factor amplitudes. In this work, the capability of the Swiss X-ray free-electron laser (SwissFEL) was used to generate large-bandwidth X-ray pulses [Δλ/λ = 2.2% full width at half-maximum (FWHM)], which were applied in SFX with the aim of improving the partiality of Bragg spots and thus decreasing sample consumption while maintaining the data quality. Sensitive data-quality indicators such as anomalous signal from native thaumatin micro-crystals and
Identifiants
pubmed: 34804544
doi: 10.1107/S2052252521008046
pii: S2052252521008046
pmc: PMC8562661
doi:
Types de publication
Journal Article
Langues
eng
Pagination
905-920Informations de copyright
© Karol Nass et al. 2021.
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