Development and Validation of a Reliable UHPLC-MS/MS Method for Simultaneous Quantification of Macrocyclic Lactones in Bovine Plasma.

Animals Cattle Chromatography, High Pressure Liquid / methods Lactones / blood Limit of Detection Macrocyclic Compounds / blood Tandem Mass Spectrometry / methods
UHPLC-MS/MS bioanalysis bovine macrocyclic lactones method development plasma

Journal

Molecules (Basel, Switzerland)
ISSN: 1420-3049
Titre abrégé: Molecules
Pays: Switzerland
ID NLM: 100964009

Informations de publication

Date de publication:
01 Feb 2022
Historique:
received: 27 12 2021
revised: 28 01 2022
accepted: 28 01 2022
entrez: 15 2 2022
pubmed: 16 2 2022
medline: 19 2 2022
Statut: epublish

Résumé

A fast, accurate and reliable ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) method was developed for simultaneous quantification of ivermectin (IVER), doramectin (DORA), and moxidectin (MOXI) in bovine plasma. A priority for sample preparation was the eradication of possible infectious diseases to avoid travel restrictions. The sample preparation was based on protein precipitation using 1% formic acid in acetonitrile, followed by Ostro

Identifiants

DOI: 10.3390/molecules27030998 PMID: 35164263 PMC: PMC8838099
pubmed: 35164263
pii: molecules27030998
doi: 10.3390/molecules27030998
pmc: PMC8838099
pii:
doi:

Substances chimiques

Lactones 0
Macrocyclic Compounds 0

Types de publication

Journal Article Validation Study

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Jimma University
ID : NASCERE_2019

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Auteurs

Gemechu Zeleke (G)

Laboratory of Pharmacology and Toxicology, Department of Pathobiology, Pharmacology and Zoological Medicine, Faculty of Veterinary Medicine, Ghent University, B-9820 Merelbeke, Belgium.
Institute of Health, School of Pharmacy, Jimma University, Jimma P.O. Box 378, Ethiopia.
ORCID: 0000-0003-4170-922X

Siegrid De Baere (S)

Laboratory of Pharmacology and Toxicology, Department of Pathobiology, Pharmacology and Zoological Medicine, Faculty of Veterinary Medicine, Ghent University, B-9820 Merelbeke, Belgium.
ORCID: 0000-0002-1382-5699

Sultan Suleman (S)

Institute of Health, School of Pharmacy, Jimma University, Jimma P.O. Box 378, Ethiopia.

Mathias Devreese (M)

Laboratory of Pharmacology and Toxicology, Department of Pathobiology, Pharmacology and Zoological Medicine, Faculty of Veterinary Medicine, Ghent University, B-9820 Merelbeke, Belgium.
ORCID: 0000-0003-2512-4176

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Classifications MeSH

questionsmedicales.fr › Eucaryotes › Animaux › Development and Validation of a Reliable...
questionsmedicales.fr › Eucaryotes › Animaux › Chordés › Vertébrés › Mammifères › Eutheria › Artiodactyla › Ruminants › Bovins › Development and Validation of a Reliable...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › Development and Validation of a Reliable...
questionsmedicales.fr › Composés chimiques organiques › Lactones › Development and Validation of a Reliable...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Statistiques comme sujet › Sensibilité et spécificité › Limite de détection › Development and Validation of a Reliable...
questionsmedicales.fr › Composés polycycliques › Composés macrocycliques › Development and Validation of a Reliable...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Development and Validation of a Reliable...