Thermoluminescence dose-response of synthesized and doped hydroxyapatite: effect of formed crystal phases.
Rietveld refinement
hydrolysis
hydrothermal
hydroxyapatite
phase transition
thermoluminescence dosimetry
Journal
Luminescence : the journal of biological and chemical luminescence
ISSN: 1522-7243
Titre abrégé: Luminescence
Pays: England
ID NLM: 100889025
Informations de publication
Date de publication:
May 2022
May 2022
Historique:
revised:
17
02
2022
received:
09
10
2021
accepted:
17
02
2022
pubmed:
22
2
2022
medline:
4
5
2022
entrez:
21
2
2022
Statut:
ppublish
Résumé
In this research work, pure and doped hydroxyapatite samples were synthesized using hydrolysis and hydrothermal methods to produce powder material. The crystal structure was carried out by producing data using the X-ray diffraction system and the Rietveld method using material analysis using diffraction software. Then the sample was irradiated with different radiation absorbed doses, and their thermoluminescence response was investigated from the dosimetry point of view. The results showed that the synthesis method, doping, and annealing temperature could significantly affect the crystal structure and thermoluminescence dosimetry response of hydroxyapatite samples, consequently. The results showed that the high-temperature annealing process and dopant could lead to the formation of the β-TCP crystal phase during or after the synthesis of hydroxyapatite, and the percentage of this formed phase increased when raising the temperature, and finally led to increase in the thermoluminescence response.
Substances chimiques
Powders
0
Durapatite
91D9GV0Z28
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
742-757Informations de copyright
© 2022 John Wiley & Sons, Ltd.
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