Fully automated measurement system for temperature-dependent X-ray total scattering at beamline BL04B2 at SPring-8.
X-ray scattering
automation
pair distribution functions
synchrotron beamline
temperature-dependence
Journal
Journal of synchrotron radiation
ISSN: 1600-5775
Titre abrégé: J Synchrotron Radiat
Pays: United States
ID NLM: 9888878
Informations de publication
Date de publication:
01 Mar 2022
01 Mar 2022
Historique:
received:
31
05
2021
accepted:
22
12
2021
entrez:
7
3
2022
pubmed:
8
3
2022
medline:
11
3
2022
Statut:
ppublish
Résumé
Data-driven approaches in materials science demand the collection of large amounts of data on the target materials at synchrotron beamlines. To accurately gather suitable experimental data, it is essential to establish fully automated measurement systems to reduce the workload of the beamline staff. Moreover, the recent COVID-19 pandemic has further emphasized the necessity of automated and/or remote measurements at synchrotron beamlines. Here, the installation of a new sample changer combined with a high-temperature furnace and a fully automated alignment system on beamline BL04B2 at SPring-8 is reported. The system allows X-ray total scattering measurements of up to 21 samples at different temperatures (from room temperature to 1200°C) to be conducted without any human assistance.
Identifiants
pubmed: 35254320
pii: S1600577521013527
doi: 10.1107/S1600577521013527
pmc: PMC8900857
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
549-554Subventions
Organisme : JSPS KAKENHI
ID : 21K14708
Informations de copyright
open access.
Références
J Synchrotron Radiat. 2015 May;22(3):675-87
pubmed: 25931084
J Appl Crystallogr. 2015 Mar 12;48(Pt 2):431-443
pubmed: 25844078
J Synchrotron Radiat. 2018 Jul 1;25(Pt 4):953-959
pubmed: 29979155
Nat Mater. 2021 Mar;20(3):274-279
pubmed: 33106651
J Synchrotron Radiat. 2012 Jan;19(Pt 1):54-9
pubmed: 22186644
Nat Commun. 2019 Jun 13;10(1):2618
pubmed: 31197134
J Appl Crystallogr. 2007 Feb 1;40(Pt 1):196-198
pubmed: 19461850
Rev Sci Instrum. 2017 Aug;88(8):085111
pubmed: 28863664