Fully Bridged Triphenylamines Comprising Five- and Seven-Membered Rings.

N-heterocycle bridged triarylamines charge transfer co-crystallization electron donor

Journal

Chemistry (Weinheim an der Bergstrasse, Germany)
ISSN: 1521-3765
Titre abrégé: Chemistry
Pays: Germany
ID NLM: 9513783

Informations de publication

Date de publication:
15 Jun 2022
Historique:
received: 02 02 2022
pubmed: 17 3 2022
medline: 17 3 2022
entrez: 16 3 2022
Statut: ppublish

Résumé

A family of fully bridged triphenylamines with embedded 5- and 7-membered rings is presented. The compounds are potent electron donors capable to undergo donor/acceptor interactions with strong cyano-based acceptors both in the solid state and solution. These interactions were evaluated by IR and UV/vis spectroscopy as well as X-ray crystallography. The vinylene-bridged compound was oxidized to the corresponding 1,2-diketone which readily underwent acid-catalyzed condensation with selected 1,2-phenylenediamines. The resulting π-extended quinoxaline derivatives represent valuable building blocks for the development of functional chromophores upon appropriate functionalization.

Identifiants

pubmed: 35293646
doi: 10.1002/chem.202200326
pmc: PMC9321823
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202200326

Subventions

Organisme : Deutsche Forschungsgemeinschaft
ID : 281029004-SFB 1249
Organisme : Deutsche Forschungsgemeinschaft
ID : 401247651-KI 1662/3-1

Informations de copyright

© 2022 The Authors. Chemistry - A European Journal published by Wiley-VCH GmbH.

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Auteurs

Ina Michalsky (I)

Organisch-Chemisches Institut, Universität Heidelberg, Im Neuenheimer Feld 270, 69120, Heidelberg, Germany.
Centre for Advanced Materials, Universität Heidelberg, Im Neuenheimer Feld 225, 69120, Heidelberg, Germany.

Viktoria Gensch (V)

Department Chemie und Pharmazie, Universität Erlangen-Nürnberg, Nikolaus-Fiebiger-Strasse 10, 91058, Erlangen, Germany.

Christian Walla (C)

Interdisziplinäres Zentrum für Wissenschaftliches Rechnen, Universität Heidelberg, Im Neuenheimer Feld 205 A, 69120, Heidelberg, Germany.

Marvin Hoffmann (M)

Interdisziplinäres Zentrum für Wissenschaftliches Rechnen, Universität Heidelberg, Im Neuenheimer Feld 205 A, 69120, Heidelberg, Germany.

Frank Rominger (F)

Organisch-Chemisches Institut, Universität Heidelberg, Im Neuenheimer Feld 270, 69120, Heidelberg, Germany.

Thomas Oeser (T)

Organisch-Chemisches Institut, Universität Heidelberg, Im Neuenheimer Feld 270, 69120, Heidelberg, Germany.

Petra Tegeder (P)

Physikalisch-Chemisches Institut, Universität Heidelberg, Im Neuenheimer Feld 253, 69120, Heidelberg, Germany.

Andreas Dreuw (A)

Interdisziplinäres Zentrum für Wissenschaftliches Rechnen, Universität Heidelberg, Im Neuenheimer Feld 205 A, 69120, Heidelberg, Germany.

Milan Kivala (M)

Organisch-Chemisches Institut, Universität Heidelberg, Im Neuenheimer Feld 270, 69120, Heidelberg, Germany.
Centre for Advanced Materials, Universität Heidelberg, Im Neuenheimer Feld 225, 69120, Heidelberg, Germany.

Classifications MeSH