Development of a multi-hormone analysis method by LC-MS/MS for environmental water application using diffusive gradient in thin films.

Chromatography, Liquid Environmental Monitoring / methods Estradiol / analysis Tandem Mass Spectrometry Water / analysis Water Pollutants, Chemical / analysis
Hormone analysis Hormones storage stability Liquid chromatography-electrospray ionisation-triple quadrupole Matrix effects Passive sampling o-DGT

Journal

Talanta
ISSN: 1873-3573
Titre abrégé: Talanta
Pays: Netherlands
ID NLM: 2984816R

Informations de publication

Date de publication:
01 Jun 2022
Historique:
received: 20 01 2022
revised: 11 03 2022
accepted: 12 03 2022
pubmed: 27 3 2022
medline: 8 4 2022
entrez: 26 3 2022
Statut: ppublish

Résumé

An analysis method for four families of hormones (estrogens, progestins, androgens and prostaglandins), dedicated to an efficient water monitoring with passive sampling, was developed using a liquid chromatography tandem mass spectrometry with triple quadrupole coupling and universal electrospray ionisation. Thirteen natural and synthetic hormones in ultra-pure water could be analysed in a single run according to the French Standard NF T90-210: calibration range of 0.1 (except for 17β-Estradiol, Estriol, Estrone and Diethylstilbestrol, from 0.5 μg/L; and Ethinylestradiol, from 1 μg/L) to 20 μg/L with linear regressions (R

Identifiants

DOI: 10.1016/j.talanta.2022.123390 PMID: 35338929
pubmed: 35338929
pii: S0039-9140(22)00186-2
doi: 10.1016/j.talanta.2022.123390
pii:
doi:

Substances chimiques

Water Pollutants, Chemical 0
Water 059QF0KO0R
Estradiol 4TI98Z838E

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

123390

Informations de copyright

Copyright © 2022 Elsevier B.V. All rights reserved.

Auteurs

Rachel Martins de Barros (R)

University of Limoges, PEIRENE, URA IRSTEA, 123 Avenue Albert Thomas, 87060, Limoges Cedex, France.

Sophie Lissalde (S)

University of Limoges, PEIRENE, URA IRSTEA, 123 Avenue Albert Thomas, 87060, Limoges Cedex, France. Electronic address: sophie.lissalde@unilim.fr.

Robin Guibal (R)

University of Limoges, PEIRENE, URA IRSTEA, 16 Rue Atlantis, 87080, Limoges Cedex, France.

Gilles Guibaud (G)

University of Limoges, PEIRENE, URA IRSTEA, 123 Avenue Albert Thomas, 87060, Limoges Cedex, France.

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Classifications MeSH

questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Development of a multi-hormone analysis method...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Pratiques en santé publique › Surveillance de l'environnement › Development of a multi-hormone analysis method...
questionsmedicales.fr › Hormones gonadiques › Hormones sexuelles stéroïdiennes › Congénères de l'oestradiol › Oestradiol › Development of a multi-hormone analysis method...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Spectrométrie de masse › Spectrométrie de masse en tandem › Development of a multi-hormone analysis method...
questionsmedicales.fr › Produits chimiques inorganiques › Composés de l'oxygène › Oxydes › Eau › Development of a multi-hormone analysis method...
questionsmedicales.fr › Actions chimiques et utilisations › Actions toxiques › Polluants environnementaux › Polluants de l'eau › Polluants chimiques de l'eau › Development of a multi-hormone analysis method...