Engineering Periodic Dinuclear Lanthanide-Directed Networks Featuring Tunable Energy Level Alignment and Magnetic Anisotropy by Metal Exchange.

X-ray magnetic circular dichroism lanthanides magnetic anisotropy metal exchange metal-organic networks scanning tunneling microscopy

Journal

Small (Weinheim an der Bergstrasse, Germany)
ISSN: 1613-6829
Titre abrégé: Small
Pays: Germany
ID NLM: 101235338

Informations de publication

Date de publication:
Jun 2022
Historique:
revised: 16 02 2022
received: 16 11 2021
pubmed: 9 4 2022
medline: 9 4 2022
entrez: 8 4 2022
Statut: ppublish

Résumé

The design of lanthanide multinuclear networks is an emerging field of research due to the potential of such materials for nanomagnetism, spintronics, and quantum information. Therefore, controlling their electronic and magnetic properties is of paramount importance to tailor the envisioned functionalities. In this work, a multidisciplinary study is presented combining scanning tunneling microscopy, scanning tunneling spectroscopy, X-ray absorption spectroscopy, X-ray linear dichroism, X-ray magnetic circular dichroism, density functional theory, and multiplet calculations, about the supramolecular assembly, electronic and magnetic properties of periodic dinuclear 2D networks based on lanthanide-pyridyl interactions on Au(111). Er- and Dy-directed assemblies feature identical structural architectures stabilized by metal-organic coordination. Notably, despite exhibiting the same +3 oxidation state, there is a shift of the energy level alignment of the unoccupied molecular orbitals between Er- and Dy-directed networks. In addition, there is a reorientation of the easy axis of magnetization and an increment of the magnetic anisotropy when the metallic center is changed from Er to Dy. Thus, the results show that it is feasible to tune the energy level alignment and magnetic anisotropy of a lanthanide-based metal-organic architecture by metal exchange, while preserving the network design.

Identifiants

pubmed: 35393751
doi: 10.1002/smll.202107073
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e2107073

Subventions

Organisme : BOREAS beamline
ID : 2020024200
Organisme : BOREAS beamline
ID : 2020094657
Organisme : Marie Sklodowska-Curie Actions
ID : 894924
Organisme : European Union's Horizon 2020
Organisme : IMDEA Nanociencia
Organisme : "Severo Ochoa" Programme for Centres of Excellence in R&D
ID : SEV-2016-0686
Organisme : European Research Council
ID : 766555
Pays : International

Informations de copyright

© 2022 The Authors. Small published by Wiley-VCH GmbH.

Références

J.-C. G. Bünzli, Acc. Chem. Res. 2006, 39, 53.
S. V. Eliseeva, J.-C. G. Bünzli, New J. Chem. 2011, 35, 1165.
J.-C. G. Bünzli, J. Coord. Chem. 2014, 67, 3706.
S. V. Eliseeva, J.-C. G. Bunzli, Chem. Soc. Rev. 2010, 39, 189.
D. N. Woodruff, R. E. P. Winpenny, R. A. Layfield, Chem. Rev. 2013, 113, 5110.
A. Gaita-Arino, H. Prima-Garcia, S. Cardona-Serra, L. Escalera-Moreno, L. E. Rosaleny, J. J. Baldovi, Inorg. Chem. Front. 2016, 3, 568.
R. Vincent, S. Klyatskaya, M. Ruben, W. Wernsdorfer, F. Balestro, Nature 2012, 488, 357.
S. Thiele, F. Balestro, R. Ballou, S. Klyatskaya, M. Ruben, W. Wernsdorfer, Science 2014, 344, 1135.
G. Aromí, F. Luis, O. Roubeau, in Lanthanides and Actinides in Molecular Magnetism, Wiley-VCH,   2015, Ch. 7.
F. Donati, S. Rusponi, S. Stepanow, C. Wäckerlin, A. Singha, L. Persichetti, R. Baltic, K. Diller, F. Patthey, E. Fernandes, J. Dreiser, Ž. Šljivančanin, K. Kummer, C. Nistor, P. Gambardella, H. Brune, Science 2016, 352, 318.
F. D. Natterer, K. Yang, W. Paul, P. Willke, T. Choi, T. Greber, A. J. Heinrich, C. P. Lutz, Nature 2017, 543, 226.
S. T. Liddle, J. van Slageren, Chem. Soc. Rev 2015, 44, 6655.
J. D. Rinehart, J. R. Long, Chem. Sci. 2011, 2, 2078.
C. Wäckerlin, F. Donati, A. Singha, R. Baltic, S. Rusponi, K. Diller, F. Patthey, M. Pivetta, Y. Lan, S. Klyatskaya, M. Ruben, H. Brune, J. Dreiser, Adv. Mater. 2016, 28, 5195.
L. Margheriti, D. Chiappe, M. Mannini, P.-E. Car, P. Sainctavit, M.-A. Arrio, F. B. de Mongeot, J. C. Cezar, F. M. Piras, A. Magnani, E. Otero, A. Caneschi, R. Sessoli, Adv. Mater. 2010, 22, 5488.
N. Ishikawa, Y. Mizuno, S. Takamatsu, T. Ishikawa, S. Koshihara, Inorg. Chem. 2008, 47, 10217.
P. Zhang, L. Zhanga, J. Tang, Dalton Trans. 2015, 44, 3923.
R. J. Blagg, L. Ungur, F. Tuna, J. Speak, P. Comar, D. Collison, W. Wernsdorfer, E. J. L. McInnes, L. F. Chibotaru, R. E. P. Winpenny, Nat. Chem. 2013, 5, 673.
R. Marin, G. Brunet, M. Murugesu, Angew. Chem., Int. Ed. 2021, 60, 1728.
J. Jiang, Y. Zhao, O. M. Yaghi, J. Am. Chem. Soc. 2016, 138, 3255.
A. E. Thorarinsdottir, T. D. Harris, Chem. Rev. 2020, 120, 8716.
L. S. Xie, G. Skorupskii, M. Dincă, Chem. Rev. 2020, 120, 8536.
J. V. Barth, G. Costantini, K. Kern, Nature 2005, 437, 671.
J. V. Barth, Annu. Rev. Phys. Chem. 2007, 58, 375.
L. Dong, Z. A. Gao, N. Lin, Prog. Surf. Sci. 2016, 91, 101.
D. Écija, J. I. Urgel, A. P. Seitsonen, W. Auwärter, J. V. Barth, Acc. Chem. Res. 2018, 51, 365.
D. Écija, J. I. Urgel, A. C. Papageorgiou, S. Joshi, W. Auwärter, A. P. Seitsonen, S. Klyatskaya, M. Ruben, S. Fischer, S. Vijayaraghavan, J. Reichert, J. V. Barth, Proc. Natl. Acad. Sci. USA. 2013, 110, 6678.
J. I. Urgel, B. Cirera, Y. Wang, W. Auwärter, R. Otero, J. M. Gallego, M. Alcamí, S. Klyatskaya, M. Ruben, F. Martin, R. Miranda, D. Ecija, J. V. Barth, Small 2015, 47, 6358.
J. I. Urgel, D. Ecija, W. Auwärter, D. Stassen, D. Bonifazi, J. V. Barth, Angew. Chem., Int. Ed. 2015, 54, 6163.
B. Cirera, L. Dordevic, R. Otero, J. M. Gallego, D. Bonifazi, R. Miranda, D. Ecija, Chem. Commun. 2016, 52, 11227.
G. Lyu, Q. Zhang, J. I. Urgel, G. Kuang, W. Auwärter, D. Ecija, J. V. Barth, N. Lin, Chem. Commun. 2016, 52, 1618.
M. Uphoff, G. S. Michelitsch, R. Hellwig, K. Reuter, H. Brune, F. Klappenberger, J. V. Barth, ACS Nano 2018, 12, 11552.
D. Moreno, B. Cirera, S. O. Parreiras, J. I. Urgel, N. Giménez-Agulló, K. Lauwaet, J. M. Gallego, J. R. Galán-Mascarós, J. I. Martínez, P. Ballester, R. Miranda, D. Écija, Chem. Commun. 2021, 57, 1380.
J. Liu, J. Li, Z. Xu, X. Zhou, Q. Xue, T. Wu, M. Zhong, R. Li, R. Sun, Z. Shen, H. Tang, S. Gao, B. Wang, S. Hou, Y. Wang, Nat. Commun. 2021, 12, 1619.
F. Klappenberger, Prog. Surf. Sci. 2014, 89, 1.
A. Singha, R. Baltic, F. Donati, C. Wäckerlin, J. Dreiser, L. Persichetti, S. Stepanow, P. Gambardella, S. Rusponi, H. Brune, Phys. Rev. B 2017, 96, 224418.
B. T. Thole, P. Carra, F. Sette, G. van der Laan, Phys. Rev. Lett. 1992, 68, 1943.
P. Carra, B. T. Thole, M. Altarelli, X. Wang, Phys. Rev. Lett. 1993, 70, 694.
A. Uldry, F. Vernay, B. Delley, Phys. Rev. B. 2012, 85, 125133.
A. Singha, F. Donati, C. Wäckerlin, R. Baltic, J. Dreiser, M. Pivetta, S. Rusponi, H. Brune, NanoLett. 2016, 16, 3475.
S. O. Parreiras, D. Moreno, B. Cirera, M. A. Valbuena, J. I. Urgel, M. Paradinas, M. Panighel, F. Ajejas, M. A. Niño, J. M. Gallego, M. Valvidares, P. Gargiani, W. Kuch, J. I. Martínez, A. Mugarza, J. Camarero, R. Miranda, P. Perna, D. Écija, Small 2021, 17, 2102753.
HyperChem(TM) Professional 7.51, Hypercube, Inc., 1115 NW 4th Street, Gainesville, Florida 32601, USA.
A. Barla, J. Nicolas, D. Cocco, S. M. Valvidares, J. Herrero-Martın, P. Gargiani, J. Moldes, C. Ruget, E. Pellegrin, S. Ferrer, J. Synchrotron Rad. 2016, 23, 1507.
Y. Teramura, A. Tanaka, B. T. Thole, T. Jo, J. Phys. Soc. Jpn. 1996, 65, 3056.
P. Giannozzi, S. Baroni, N. Bonini, M. Calandra, R. Car, C. Cavazzoni, D. Ceresoli, G. L. Chiarotti, M. Cococcioni, I. Dabo, A. Dal Corso, S. de Gironcoli, S. Fabris, G. Fratesi, R. Gebauer, U. Gerstmann, C. Gougoussis, A. Kokalj, M. Lazzeri, L. Martin-Samos, N. Marzari, F. Mauri, R. Mazzarello, S. Paolini, A. Pasquarello, L. Paulatto, C. Sbraccia, S. Scandolo, G. Sclauzero, A. P. Seitsonen, et al., J. Phys.: Condens. Matter 2009, 21, 395502.
L. A. Constantin, J. P. Perdew, J. M. Pitarke, Phys. Rev. B 2009, 79, 075126.
J. P. Perdew, A. Ruzsinszky, G. I. Csonka, O. A. Vydrov, G. E. Scuseria, L. A. Constantin, X. Zhou, K. Burke, Phys. Rev. Lett. 2008, 100, 136406.
G. Kresse, J. Joubert, Phys. Rev. B 1999, 59, 1758.
J. D. Pack, H. J. Monkhorst, Phys. Rev. B 1977, 16, 1748.
S. Grimme, J. Antony, S. Ehrlich, H. Krieg, J. Chem. Phys. 2010, 132, 154104.
M. Methfessel, A. T. Paxton, Phys. Rev. B 1989, 40, 3616.

Auteurs

Daniel Moreno (D)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Sofia O Parreiras (SO)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

José I Urgel (JI)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Beatriz Muñiz-Cano (B)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Cristina Martín-Fuentes (C)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Koen Lauwaet (K)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Manuel Valvidares (M)

ALBA Synchrotron Light Source, Cerdanyola del Vallès, 08290, Spain.

Miguel A Valbuena (MA)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

José M Gallego (JM)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.
Instituto de Ciencia de Materiales de Madrid (ICMM-CSIC), Cantoblanco, Madrid, 28049, Spain.

José I Martínez (JI)

Instituto de Ciencia de Materiales de Madrid (ICMM-CSIC), Cantoblanco, Madrid, 28049, Spain.

Pierluigi Gargiani (P)

ALBA Synchrotron Light Source, Cerdanyola del Vallès, 08290, Spain.

Julio Camarero (J)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.
Departamento de Física de la Materia Condensada and Condensed Matter Physics Center (IFIMAC), Universidad Autónoma de Madrid, Cantoblanco, Madrid, 28049, Spain.

Rodolfo Miranda (R)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.
Departamento de Física de la Materia Condensada and Condensed Matter Physics Center (IFIMAC), Universidad Autónoma de Madrid, Cantoblanco, Madrid, 28049, Spain.

David Écija (D)

Instituto Madrileño de Estudios Avanzados en Nanociencia (IMDEA Nanoscience), Madrid, 28049, Spain.

Classifications MeSH