Fluorescent bioassay for SARS-CoV-2 detection using polypyrene-g-poly(ε-caprolactone) prepared by simultaneous photoinduced step-growth and ring-opening polymerizations.

Fluorescent biosensor Graft copolymer Photopolymerization Ring-opening polymerization SARS-CoV-2 Step-growth polymerization

Journal

Mikrochimica acta
ISSN: 1436-5073
Titre abrégé: Mikrochim Acta
Pays: Austria
ID NLM: 7808782

Informations de publication

Date de publication:
26 04 2022
Historique:
received: 11 01 2022
accepted: 22 02 2022
entrez: 27 4 2022
pubmed: 28 4 2022
medline: 29 4 2022
Statut: epublish

Résumé

The construction of a rapid and easy immunofluorescence bioassay for SARS-CoV-2 detection is described. We report for the first time a novel one-pot synthetic approach for simultaneous photoinduced step-growth polymerization of pyrene (Py) and ring-opening polymerization of ε-caprolactone (PCL) to produce a graft fluorescent copolymer PPy-g-PCL that was conjugated to SARS-CoV-2-specific antibodies using EDC/NHS chemistry. The synthesis steps and conjugation products were fully characterized using standard spectral analysis. Next, the PPy-g-PCL was used for the construction of a dot-blot assay which was calibrated for applications to human nasopharyngeal samples. The analytical features of the proposed sensor showed a detection range of 6.03-8.7 LOG viral copy mL

Identifiants

pubmed: 35474492
doi: 10.1007/s00604-022-05244-2
pii: 10.1007/s00604-022-05244-2
pmc: PMC9042169
doi:

Substances chimiques

Caproates 0
Coloring Agents 0
Lactones 0
Polyesters 0
Poly A 24937-83-5
polycaprolactone 24980-41-4
caprolactone 56RE988L1R

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

202

Subventions

Organisme : The Scientific and Technological Research Council of Turkey
ID : 120C121
Organisme : Bilimsel Araştirma Projeleri Birimi, Istanbul Üniversitesi
ID : TUB-2021-43195
Organisme : Ege Üniversitesi
ID : TOA-2020-21862

Informations de copyright

© 2022. The Author(s), under exclusive licence to Springer-Verlag GmbH Austria, part of Springer Nature.

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Auteurs

Tugba Celiker (T)

Department of Chemistry, Istanbul Technical University, 34469, Maslak, Istanbul, Turkey.

Faezeh Ghorbanizamani (F)

Department of Biochemistry, Faculty of Science, Ege University, 35100, Bornova, Izmir, Turkey.

Hichem Moulahoum (H)

Department of Biochemistry, Faculty of Science, Ege University, 35100, Bornova, Izmir, Turkey.

Emine Guler Celik (E)

Department of Bioengineering, Faculty of Engineering, Ege University, 35100, Bornova, Izmir, Turkey. emine.guler.celik@ege.edu.tr.

Kerem Tok (K)

Department of Biochemistry, Faculty of Science, Ege University, 35100, Bornova, Izmir, Turkey.

Figen Zihnioglu (F)

Department of Biochemistry, Faculty of Science, Ege University, 35100, Bornova, Izmir, Turkey.

Candan Cicek (C)

Department of Medical Microbiology, Faculty of Medicine, Ege University, 35100, Bornova, Izmir, Turkey.

Ruchan Sertoz (R)

Department of Medical Microbiology, Faculty of Medicine, Ege University, 35100, Bornova, Izmir, Turkey.

Bilgin Arda (B)

Department of Infectious Diseases and Clinical Microbiology, Faculty of Medicine, Ege University, 35100, Bornova, Izmir, Turkey.

Tuncay Goksel (T)

Department of Pulmonary Medicine, Faculty of Medicine, Ege University, 35100, Bornova, Izmir, Turkey.
EGESAM-Ege University Translational Pulmonary Research Center, 35100, Bornova, Izmir, Turkey.

Kutsal Turhan (K)

Department of Thoracic Surgery, Faculty of Medicine, Ege University, 35100, Bornova, Izmir, Turkey.

Suna Timur (S)

Department of Biochemistry, Faculty of Science, Ege University, 35100, Bornova, Izmir, Turkey.
Central Research Test and Analysis Laboratory Application and Research Center, Ege University, 35100, Bornova, Izmir, Turkey.

Yusuf Yagci (Y)

Department of Chemistry, Istanbul Technical University, 34469, Maslak, Istanbul, Turkey. yusuf@itu.edu.tr.
Faculty of Science, Chemistry Department, King Abdulaziz University, Jeddah, 21589, Saudi Arabia. yusuf@itu.edu.tr.

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Classifications MeSH