Efficient Synthesis of Various Substituted (Thio)Ureas, Semicarbazides, Thiosemicarbazides, Thiazolidones, and Oxadiazole Derived from [2.2]Paracyclophane.
Journal
ACS omega
ISSN: 2470-1343
Titre abrégé: ACS Omega
Pays: United States
ID NLM: 101691658
Informations de publication
Date de publication:
19 Apr 2022
19 Apr 2022
Historique:
received:
07
01
2022
accepted:
23
02
2022
entrez:
27
4
2022
pubmed:
28
4
2022
medline:
28
4
2022
Statut:
epublish
Résumé
The strategies of the syntheses of various (thio)ureas, semicarbazides, thiosemicarbazides, thiazolidones, and oxadiazole derived from the [2.2]paracyclophane molecule are achieved starting with 4-(2.2]paracyclophanyl)isocyanate. The structures of the obtained products were elucidated by NMR, mass spectrometry, and infrared (IR) spectroscopy in addition to high-resolution mass spectrometry (HRMS). X-ray structure analysis was also used to prove the assigned structure.
Identifiants
pubmed: 35474844
doi: 10.1021/acsomega.2c00141
pmc: PMC9026011
doi:
Types de publication
Journal Article
Langues
eng
Pagination
12879-12890Informations de copyright
© 2022 The Authors. Published by American Chemical Society.
Déclaration de conflit d'intérêts
The authors declare no competing financial interest.
Références
Molecules. 2016 Jan 23;21(2):138
pubmed: 26805812
Chem Cent J. 2017 Apr 7;11(1):32
pubmed: 29086809
Eur J Med Chem. 2006 Jan;41(1):80-7
pubmed: 16300859
Molecules. 2020 Jul 22;25(15):
pubmed: 32707754
Acta Crystallogr A Found Adv. 2015 Jan;71(Pt 1):3-8
pubmed: 25537383
Eur J Med Chem. 2003 Jul-Aug;38(7-8):781-6
pubmed: 12932910
Angew Chem Int Ed Engl. 2003 Mar 17;42(11):1210-50
pubmed: 12645054
Eur J Med Chem. 2008 Nov;43(11):2347-53
pubmed: 18313806
Molecules. 2020 Jul 28;25(15):
pubmed: 32731576
Eur J Med Chem. 2010 Apr;45(4):1323-31
pubmed: 20056520
Beilstein J Org Chem. 2015 Apr 07;11:437-45
pubmed: 25977718
Molecules. 2020 Nov 27;25(23):
pubmed: 33260954
Chem Soc Rev. 2018 Sep 17;47(18):6947-6963
pubmed: 30065985
Org Biomol Chem. 2003 Apr 21;1(8):1256-69
pubmed: 12929653
Acta Crystallogr C Struct Chem. 2015 Jan;71(Pt 1):3-8
pubmed: 25567568
Bioorg Med Chem. 2009 Mar 1;17(5):1957-62
pubmed: 19217789