An Improved GC-MS Method for Malondialdehyde (MDA) Detection: Avoiding the Effects of Nitrite in Foods.

GC-MS lipid peroxidation malondialdehyde nitrite pickled products

Journal

Foods (Basel, Switzerland)
ISSN: 2304-8158
Titre abrégé: Foods
Pays: Switzerland
ID NLM: 101670569

Informations de publication

Date de publication:
19 Apr 2022
Historique:
received: 25 02 2022
revised: 02 04 2022
accepted: 15 04 2022
entrez: 14 5 2022
pubmed: 15 5 2022
medline: 15 5 2022
Statut: epublish

Résumé

Malondialdehyde (MDA) is one of the representative end products under lipid peroxidation, indicating the degree of lipid oxidation in foods. However, compounds in pickled products, especially the nitrite in salted lean pork can react with MDA under the acidic condition, leads to the loss of MDA and an underestimation on lipid oxidation through the conventional assay. In this study, the quantification for MDA in the sample containing sodium nitrite were found lacking accuracy by the thiobarbituric acid (TBA) assay and chromatography assay based on alkaline hydrolysis as the reaction between them were difficult to be completely inhibited. Among other trials, the improvement GC-MS analysis utilizing deuterium substituted MDA (MDA-d

Identifiants

pubmed: 35563899
pii: foods11091176
doi: 10.3390/foods11091176
pmc: PMC9099496
pii:
doi:

Types de publication

Journal Article

Langues

eng

Subventions

Organisme : the National Natural Science Foundation of China
ID : No. 31871869
Organisme : the National Key R&D Program of China
ID : No. 2018YFD0901006

Références

Food Chem. 2019 Nov 15;298:125009
pubmed: 31260970
Anal Chim Acta. 2008 Feb 25;609(2):175-83
pubmed: 18261512
Compr Rev Food Sci Food Saf. 2020 Mar;19(2):503-529
pubmed: 33325172
Rapid Commun Mass Spectrom. 2014 Dec 30;28(24):2723-8
pubmed: 25380494
J Chromatogr A. 2016 Mar 11;1437:241-246
pubmed: 26879451
J Pharm Biomed Anal. 2007 Jan 17;43(2):619-24
pubmed: 16949242
J Agric Food Chem. 2012 Sep 26;60(38):9589-94
pubmed: 22950760
Food Chem. 2016 Oct 15;209:90-4
pubmed: 27173538
J Agric Food Chem. 2005 Jun 15;53(12):4708-13
pubmed: 15941304
J Chromatogr B Analyt Technol Biomed Life Sci. 2003 Mar 5;785(2):337-44
pubmed: 12554147
J Agric Food Chem. 2017 Dec 27;65(51):11320-11328
pubmed: 29179555
J Chromatogr B Analyt Technol Biomed Life Sci. 2017 Feb 1;1043:167-175
pubmed: 27461359
Anal Biochem. 2005 Mar 1;338(1):62-70
pubmed: 15707936
J Pharm Biomed Anal. 2007 Jan 17;43(2):701-7
pubmed: 16959461
Chromatographia. 2012 May;75(9-10):433-440
pubmed: 22593603
Anal Biochem. 2017 May 1;524:31-44
pubmed: 27530652
Anal Biochem. 2017 May 1;524:13-30
pubmed: 27789233
Biomed Chromatogr. 2015 Jan;29(1):41-6
pubmed: 25355691
Mass Spectrom Rev. 2011 May-Jun;30(3):491-509
pubmed: 21500246
Antioxidants (Basel). 2019 Sep 25;8(10):
pubmed: 31557858
Free Radic Res. 2013 Aug;47(8):651-6
pubmed: 23745592
Rapid Commun Mass Spectrom. 2015 Jun 15;29(11):1069-79
pubmed: 26044275
J Chromatogr B Analyt Technol Biomed Life Sci. 2016 Apr 15;1019:95-111
pubmed: 26522895
Meat Sci. 2014 Dec;98(4):569-73
pubmed: 25089778

Auteurs

Wenjie Wang (W)

College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China.
Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China.
National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China.
Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China.

Zhiwen Zhang (Z)

College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China.
Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China.
National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China.
Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China.

Xiaoying Liu (X)

College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China.
Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China.
National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China.
Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China.

Xiaoji Cao (X)

Research Center of Analysis and Measurement, Zhejiang University of Technology, Hangzhou 310014, China.

Lianzhu Wang (L)

Yellow Sea Fisheries Research Institute, Chinese Academy of Fishery Sciences, Qingdao 266071, China.

Yuting Ding (Y)

College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China.
Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China.
National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China.
Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China.

Xuxia Zhou (X)

College of Food Science and Technology, Zhejiang University of Technology, Hangzhou 310014, China.
Key Laboratory of Marine Fishery Resources Exploitment & Utilization of Zhejiang Province, Hangzhou 310014, China.
National R&D Branch Center for Pelagic Aquatic Products Processing (Hangzhou), Hangzhou 310014, China.
Collaborative Innovation Center of Seafood Deep Processing, Dalian Polytechnic University, Dalian 116034, China.

Classifications MeSH