Ultra-high vacuum cleaver for the preparation of ionic crystal surfaces.


Journal

The Review of scientific instruments
ISSN: 1089-7623
Titre abrégé: Rev Sci Instrum
Pays: United States
ID NLM: 0405571

Informations de publication

Date de publication:
01 May 2022
Historique:
entrez: 1 6 2022
pubmed: 2 6 2022
medline: 2 6 2022
Statut: ppublish

Résumé

Cleaving single crystals in situ under ultra-high vacuum conditions provides a reliable and straightforward approach to prepare clean and atomically well-defined surfaces. Here, we present a versatile sample cleaver to efficiently prepare ionic crystal surfaces under ultra-high vacuum conditions, which is suitable for preparation of softer materials, such as alkali halides, and harder materials, such as metal oxides. One of the advantages of the presented cleaver design is that the cleaving blade and anvil to support the crystal are incorporated into the device. Therefore, no particularly strong mechanical manipulator is needed, and it is compatible with existing vacuum chambers equipped with an xyz-manipulator. We demonstrate atomically flat terraces and the atomic structure of NaCl(001), KBr(001), NiO(001), and MgO(001) cleavage planes prepared in situ under ultra-high vacuum conditions and imaged by low-temperature non-contact atomic force microscopy.

Identifiants

pubmed: 35649805
doi: 10.1063/5.0088802
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

053703

Auteurs

Tim Sander (T)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Yi Liu (Y)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Tuan Anh Pham (TA)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Maximilian Ammon (M)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Mirunalini Devarajulu (M)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Sabine Maier (S)

Department of Physics, Friedrich-Alexander-Universität Erlangen-Nürnberg, Erwin-Rommel-Straße 1, 91058 Erlangen, Germany.

Classifications MeSH