Optimal self-assembly of lipid nanoparticles (LNP) in a ring micromixer.


Journal

Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288

Informations de publication

Date de publication:
08 06 2022
Historique:
received: 09 02 2022
accepted: 20 05 2022
entrez: 8 6 2022
pubmed: 9 6 2022
medline: 11 6 2022
Statut: epublish

Résumé

Lipid nanoparticles (LNPs) for RNA and DNA delivery have attracted considerable attention for their ability to treat a broad range of diseases and to vectorize mRNA for COVID vaccines. LNPs are produced by mixing biomolecules and lipids, which self-assemble to form the desired structure. In this domain, microfluidics shows clear advantages: high mixing quality, low-stress conditions, and fast preparation. Studies of LNPs produced in micromixers have revealed, in certain ranges of flow rates, a degradation in performance in terms of size, monodispersity and encapsulation efficiency. In this study, we focus on the ring micromixer, which is well adapted to high throughput. We reveal three regimes, side-by-side, transitional and highly mixed, that control the mixing performance of the device. Furthermore, using cryo-TEM and biochemical analysis, we show that the mixing performances are strongly correlated to the characteristics of the LNPs we produce. We emphasize the importance of the flow-rate ratio and propose a physical criterion based on the onset of temporal instabilities for producing LNPs with optimal characteristics in terms of geometry, monodispersity and encapsulation yield. These criteria are generally applicable.

Identifiants

pubmed: 35676394
doi: 10.1038/s41598-022-13112-5
pii: 10.1038/s41598-022-13112-5
pmc: PMC9177731
doi:

Substances chimiques

Lipid Nanoparticles 0
Lipids 0
Liposomes 0
RNA, Small Interfering 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

9483

Informations de copyright

© 2022. The Author(s).

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Auteurs

Manon Ripoll (M)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Elian Martin (E)

Microfluidics, MEMS, Nanostructures Laboratory, CNRS Chimie Biologie Innovation (CBI), UMR 8231, Institut Pierre Gilles de Gennes (IPGG), ESPCI Paris, PSL Research University, 6 rue Jean Calvin, 75005, Paris, France.

Mathilde Enot (M)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Oscar Robbe (O)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Chiara Rapisarda (C)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Marie-Claire Nicolai (MC)

REI Department, SANOFI Pasteur, 1541 Av. Marcel Mérieux, 69280, Marcy-L'Étoile, France.

Aurélie Deliot (A)

REI Department, SANOFI Pasteur, 1541 Av. Marcel Mérieux, 69280, Marcy-L'Étoile, France.

Patrick Tabeling (P)

Microfluidics, MEMS, Nanostructures Laboratory, CNRS Chimie Biologie Innovation (CBI), UMR 8231, Institut Pierre Gilles de Gennes (IPGG), ESPCI Paris, PSL Research University, 6 rue Jean Calvin, 75005, Paris, France. ptabeling30@gmail.com.

Jean-René Authelin (JR)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Mostafa Nakach (M)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

Pierre Wils (P)

BioDPD Department, SANOFI, 13 Quai Jules Guesde, 94400, Vitry-sur-Seine, France.

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Classifications MeSH