A Versatile Chemoenzymatic Nanoreactor that Mimics NAD(P)H Oxidase for the In Situ Regeneration of Cofactors.


Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
26 09 2022
Historique:
received: 11 05 2022
pubmed: 29 6 2022
medline: 23 9 2022
entrez: 28 6 2022
Statut: ppublish

Résumé

Herein, we report a multifunctional chemoenzymatic nanoreactor (NanoNOx) for the glucose-controlled regeneration of natural and artificial nicotinamide cofactors. NanoNOx are built of glucose oxidase-polymer hybrids that assemble in the presence of an organometallic catalyst: hemin. The design of the hybrid is optimized to increase the effectiveness and the directional channeling at low substrate concentration. Importantly, NanoNOx can be reutilized without affecting the catalytic properties, can show high stability in the presence of organic solvents, and can effectively oxidize assorted natural and artificial enzyme cofactors. Finally, the hybrid was successfully coupled with NADH-dependent dehydrogenases in one-pot reactions, using a strategy based on the sequential injection of a fuel, namely, glucose. Hence, this study describes the first example of a hybrid chemoenzymatic nanomaterial able to efficiently mimic NOx enzymes in cooperative one-pot cascade reactions.

Identifiants

pubmed: 35762738
doi: 10.1002/anie.202206926
pmc: PMC9796410
doi:

Substances chimiques

Coenzymes 0
Polymers 0
Solvents 0
NAD 0U46U6E8UK
Niacinamide 25X51I8RD4
Hemin 743LRP9S7N
Oxidoreductases EC 1.-
Glucose Oxidase EC 1.1.3.4
NADPH Oxidases EC 1.6.3.-
Glucose IY9XDZ35W2

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202206926

Informations de copyright

© 2022 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Andoni Rodriguez-Abetxuko (A)

CIC nanoGUNE, Basque Research and Technology Alliance (BRTA), Tolosa Hiribidea 76, 20018, Donostia-San Sebastián, Spain.

Antonio Reifs (A)

CIC nanoGUNE, Basque Research and Technology Alliance (BRTA), Tolosa Hiribidea 76, 20018, Donostia-San Sebastián, Spain.

Daniel Sánchez-deAlcázar (D)

POLYMAT and Department of Applied Chemistry, University of the Basque Country UPV/EHU, Paseo Manuel Lardizabal 3, 20018, Donostia-San Sebastián, Spain.

Ana Beloqui (A)

POLYMAT and Department of Applied Chemistry, University of the Basque Country UPV/EHU, Paseo Manuel Lardizabal 3, 20018, Donostia-San Sebastián, Spain.
IKERBASQUE, Plaza Euskadi 5, 48009, Bilbao, Spain.

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Classifications MeSH