From target analysis to suspect and non-target screening of endocrine-disrupting compounds in human urine.
Endocrine-disrupting compounds
High-resolution tandem mass spectrometry
Liquid chromatography tandem mass spectrometry
Suspect and non-target screening
Target analysis
Journal
Analytical and bioanalytical chemistry
ISSN: 1618-2650
Titre abrégé: Anal Bioanal Chem
Pays: Germany
ID NLM: 101134327
Informations de publication
Date de publication:
Sep 2022
Sep 2022
Historique:
received:
30
05
2022
accepted:
22
07
2022
revised:
14
07
2022
pubmed:
30
7
2022
medline:
8
9
2022
entrez:
29
7
2022
Statut:
ppublish
Résumé
In the present work, a target analysis method for simultaneously determining 24 diverse endocrine-disrupting compounds (EDCs) in urine (benzophenones, bisphenols, parabens, phthalates and antibacterials) was developed. The target analysis approach (including enzymatic hydrolysis, clean-up by solid-phase extraction and analysis by liquid chromatography coupled to tandem mass spectrometry (LC-MS/MS)) was optimized, validated and applied to volunteers' samples, in which 67% of the target EDCs were quantified. For instance, benzophenone-3 (0.2-13 ng g
Identifiants
pubmed: 35904524
doi: 10.1007/s00216-022-04250-w
pii: 10.1007/s00216-022-04250-w
pmc: PMC9436830
doi:
Substances chimiques
Benzhydryl Compounds
0
Endocrine Disruptors
0
Parabens
0
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
6855-6869Subventions
Organisme : Ministerio de Ciencia e Innovación
ID : PID2020-117686RB-C31
Organisme : Eusko Jaurlaritza
ID : IT1213-19
Informations de copyright
© 2022. The Author(s).
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