In situ discrimination of polymorphs and phase transformation of sulfamerazine using quartz crystal microbalance.

Crystallization Quartz Quartz Crystal Microbalance Techniques Sulfamerazine / chemistry
Polymorph discrimination QCM Selective nucleation Surface modification

Journal

Analytica chimica acta
ISSN: 1873-4324
Titre abrégé: Anal Chim Acta
Pays: Netherlands
ID NLM: 0370534

Informations de publication

Date de publication:
15 Aug 2022
Historique:
received: 13 02 2022
revised: 21 05 2022
accepted: 28 06 2022
entrez: 7 8 2022
pubmed: 8 8 2022
medline: 10 8 2022
Statut: ppublish

Résumé

A novel strategy utilizing the quartz crystal microbalance (QCM) was developed for the in situ discrimination of polymorphic nucleation (form-I and form-II) and phase transformation of sulfamerazine (SMZ) in cooling crystallization. According to Ostwald's rule of stages, metastable form-I of SMZ is first nucleated and then shifted to stable form-II by solution-mediated phase transformation. Through surface modification with the self-assembled monolayer technique of a functional group, QCM distinctively detects the formation of the two polymorphs. The results indicated that -NH

Identifiants

DOI: 10.1016/j.aca.2022.340137 PMID: 35934408
pubmed: 35934408
pii: S0003-2670(22)00708-5
doi: 10.1016/j.aca.2022.340137
pii:
doi:

Substances chimiques

Quartz 14808-60-7
Sulfamerazine UR1SAB295F

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

340137

Informations de copyright

Copyright © 2022 Elsevier B.V. All rights reserved.

Auteurs

Li-Shang Liu (LS)

Shandong Provincial Key Laboratory of Detection Technology of Tumor Markers, College of Chemistry and Chemical Engineering, Linyi University, Linyi, 276005, PR China; Functional Crystallization Center, Department of Chemical Engineering (Integrated Engineering Program), Kyung Hee University, Yongin-si, Gyeonggi-do, 446-701, South Korea.

Jong-Min Kim (JM)

Department of Chemical Eng., Dong-A University, Hadan 840, Saha, Busan, 604-741, South Korea. Electronic address: jmkim3@dau.ac.kr.

Woo-Sik Kim (WS)

Functional Crystallization Center, Department of Chemical Engineering (Integrated Engineering Program), Kyung Hee University, Yongin-si, Gyeonggi-do, 446-701, South Korea. Electronic address: wskim@khu.ac.kr.

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Classifications MeSH

questionsmedicales.fr › Phénomènes chimiques › Cristallisation › In situ discrimination of polymorphs and phase...
questionsmedicales.fr › Produits chimiques inorganiques › Composés du silicium › Silice › Quartz › In situ discrimination of polymorphs and phase...
questionsmedicales.fr › Techniques d'investigation › Poids et mesures › Techniques de microbalance à cristal de quartz › In situ discrimination of polymorphs and phase...
questionsmedicales.fr › Composés chimiques organiques › Composés du soufre › Sulfones › Sulfonamides › Sulfamides › Sulfamérazine › In situ discrimination of polymorphs and phase...