Imaging Cu
Journal
Nature communications
ISSN: 2041-1723
Titre abrégé: Nat Commun
Pays: England
ID NLM: 101528555
Informations de publication
Date de publication:
29 Aug 2022
29 Aug 2022
Historique:
received:
18
01
2022
accepted:
22
07
2022
entrez:
29
8
2022
pubmed:
30
8
2022
medline:
30
8
2022
Statut:
epublish
Résumé
Understanding morphological changes of nanoparticles in solution is essential to tailor the functionality of devices used in energy generation and storage. However, we lack experimental methods that can visualize these processes in solution, or in electrolyte, and provide three-dimensional information. Here, we show how X-ray ptychography enables in situ nano-imaging of the formation and hollowing of nanoparticles in solution at 155 °C. We simultaneously image the growth of about 100 nanocubes with a spatial resolution of 66 nm. The quantitative phase images give access to the third dimension, allowing to additionally study particle thickness. We reveal that the substrate hinders their out-of-plane growth, thus the nanocubes are in fact nanocuboids. Moreover, we observe that the reduction of Cu
Identifiants
pubmed: 36038564
doi: 10.1038/s41467-022-32373-2
pii: 10.1038/s41467-022-32373-2
pmc: PMC9424245
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
4971Subventions
Organisme : EC | EU Framework Programme for Research and Innovation H2020 | H2020 Priority Excellent Science | H2020 European Research Council (H2020 Excellent Science - European Research Council)
ID : 818941
Organisme : Deutsche Forschungsgemeinschaft (German Research Foundation)
ID : EXC 788 2056 - project ID 390715994.
Organisme : Bundesministerium für Bildung und Forschung (Federal Ministry of Education and Research)
ID : Röntgen-Ångström-Cluster via the project 05K2020 - 2019-06104 XStereoVision
Informations de copyright
© 2022. The Author(s).
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