Hydrothermal synthesis of multi-cationic high-entropy layered double hydroxides.


Journal

RSC advances
ISSN: 2046-2069
Titre abrégé: RSC Adv
Pays: England
ID NLM: 101581657

Informations de publication

Date de publication:
12 Sep 2022
Historique:
received: 30 08 2022
accepted: 31 08 2022
entrez: 24 10 2022
pubmed: 25 10 2022
medline: 25 10 2022
Statut: epublish

Résumé

High-entropy materials are compositionally complex materials which often contain five or more elements. The most commonly studied materials in this field are alloys and oxides, where their composition allows for tunable materials properties. High-entropy layered double hydroxides have been recently touted as the next focus for the field of high-entropy materials to expand into. However, most previous work on multi-cationic layered double hydroxides has focused on syntheses with 5 or less cations in the structure. To bridge this gap into high-entropy materials, this work explores the range and extent of different compositional combinations for high-entropy double layered hydroxides. Specifically, pure layered double hydroxides were synthesized with different combinations of 7 cations (Mg, Co, Cu, Zn, Ni, Al, Fe, Cr) as well as one combination of 8 cations by utilizing a hydrothermal synthesis method. Furthermore, magnetic properties of the 8-cation LDH were investigated.

Identifiants

pubmed: 36275118
doi: 10.1039/d2ra05435c
pii: d2ra05435c
pmc: PMC9475562
doi:

Types de publication

Journal Article

Langues

eng

Pagination

26362-26371

Informations de copyright

This journal is © The Royal Society of Chemistry.

Déclaration de conflit d'intérêts

There are no conflicts to declare.

Références

Nat Commun. 2015 Sep 29;6:8485
pubmed: 26415623
Chem Soc Rev. 2014;43(20):7040-66
pubmed: 25001024
Inorg Chem. 2018 Oct 15;57(20):13027-13033
pubmed: 30256098
J Am Chem Soc. 2020 Mar 11;142(10):4550-4554
pubmed: 32105461
Chem Rev. 2012 Jul 11;112(7):4124-55
pubmed: 22452296
Sci Rep. 2021 Aug 12;11(1):16403
pubmed: 34385486
Phys Rev Lett. 2001 Jan 22;86(4):720-3
pubmed: 11177921
J Synchrotron Radiat. 2005 Jul;12(Pt 4):537-41
pubmed: 15968136
Sci Rep. 2018 Jun 5;8(1):8609
pubmed: 29872126
Sci Rep. 2016 Nov 29;6:37946
pubmed: 27897255

Auteurs

Amy J Knorpp (AJ)

Laboratory for High Performance Ceramics, Empa. Swiss Federal Laboratories for Materials Science and Technology Überlandstrasse 129 CH-8600 Dübendorf Switzerland amy.knorpp@empa.ch michael.stuer@empa.ch.

Anna Zawisza (A)

Laboratory for High Performance Ceramics, Empa. Swiss Federal Laboratories for Materials Science and Technology Überlandstrasse 129 CH-8600 Dübendorf Switzerland amy.knorpp@empa.ch michael.stuer@empa.ch.
Department of Ceramics and Refractories, Faculty of Materials Science and Ceramics, AGH University of Science and Technology al. Mickiewicza 30-059 Krakow Poland.

Shangxiong Huangfu (S)

Laboratory for High Performance Ceramics, Empa. Swiss Federal Laboratories for Materials Science and Technology Überlandstrasse 129 CH-8600 Dübendorf Switzerland amy.knorpp@empa.ch michael.stuer@empa.ch.

Aurelio Borzì (A)

Center for X-ray Analytics, Swiss Federal Laboratories for Materials Science and Technology Empa. Überlandstrasse 129 CH-8600 Dübendorf Switzerland.

Adam H Clark (AH)

Energy and Environment Division, Paul Scherrer Insitut Forschungsstrasse 111 5232 Villigen PSI Switzerland.

Dariusz Kata (D)

Department of Ceramics and Refractories, Faculty of Materials Science and Ceramics, AGH University of Science and Technology al. Mickiewicza 30-059 Krakow Poland.

Thomas Graule (T)

Laboratory for High Performance Ceramics, Empa. Swiss Federal Laboratories for Materials Science and Technology Überlandstrasse 129 CH-8600 Dübendorf Switzerland amy.knorpp@empa.ch michael.stuer@empa.ch.

Michael Stuer (M)

Laboratory for High Performance Ceramics, Empa. Swiss Federal Laboratories for Materials Science and Technology Überlandstrasse 129 CH-8600 Dübendorf Switzerland amy.knorpp@empa.ch michael.stuer@empa.ch.

Classifications MeSH