Multiscale Reciprocal Space Mapping of Magnetite Mesocrystals.
magnetite
mesocrystals
microscopic structure
multiple-length-scale structures
supercrystallography
Journal
Advanced materials (Deerfield Beach, Fla.)
ISSN: 1521-4095
Titre abrégé: Adv Mater
Pays: Germany
ID NLM: 9885358
Informations de publication
Date de publication:
Jan 2023
Jan 2023
Historique:
revised:
04
10
2022
received:
05
08
2022
pubmed:
29
10
2022
medline:
29
10
2022
entrez:
28
10
2022
Statut:
ppublish
Résumé
Mesocrystals are a class of nanostructured material, where a multiple-length-scale structure is a prerequisite of many interesting phenomena. Resolving the mesocrystal structure is quite challenging due to their structuration on different length scales. The combination of small- and wide-angle X-ray scattering (SAXS and WAXS) techniques offers the possibility of non-destructively probing mesocrystalline structures simultaneously, over multiple length scales to reveal their microscopic structure. This work describes how high dynamical range of modern detectors sheds light on the weak features of scattering, significantly increasing the information content. The detailed analysis of X-ray diffraction (XRD) from the magnetite mesocrystals with different particle sizes and shapes is described, in tandem with electron microscopy. The revealed features provide valuable input to the models of mesocrystal growth and the choice of structural motif; the impact on magnetic properties is discussed.
Identifiants
pubmed: 36305045
doi: 10.1002/adma.202207130
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
e2207130Subventions
Organisme : Deutsche Forschungsgemeinschaft
Organisme : Horizon 2020 research and innovation program of the European Union
ID : 715620
Organisme : European Research Council
Pays : International
Informations de copyright
© 2022 The Authors. Advanced Materials published by Wiley-VCH GmbH.
Références
a) H. Cölfen, M. Antonietti, Mesocrystals and Nonclassical Crystallization, Wiley, Chichester, UK 2008;
b) E. V. Sturm, H. Cölfen, Crystals 2017, 7, 207;
c) E. V. Sturm, H. Cölfen, Chem. Soc. Rev. 2016, 45, 5821.
L. Bergström, E. V. Sturm, G. Salazar-Alvarez, H. Cölfen, Acc. Chem. Res. 2015, 48, 1391.
a) J. Fang, B. Ding, H. Gleiter, Chem. Soc. Rev. 2011, 40, 5347;
b) T. Tachikawa, T. Majima, NPG Asia Mater. 2014, 6, 100.
L. Bahrig, S. G. Hickey, A. Eychmüller, CrystEngComm 2014, 16, 9408.
E. Uchaker, G. Cao, Nano Today 2014, 9, 499.
L. Zhou, P. O'Brien, J. Phys. Chem. Lett. 2012, 3, 620.
a) M. E. Fleet, Acta Crystallogr B 1981, 37, 917;
b) R. M. Cornell, U. Schwertmann, The Iron Oxides: Structure, Properties, Reactions, Occurrences and Uses, Wiley-VCH, Weinheim, Germany 2003.
C. Kittel, P. McEuen, Introduction to Solid State Physics, John Wiley & Sons, Hoboken, NJ, USA 2018.
J. Frenkel, J. Doefman, Nature 1930, 126, 274.
a) R. Yanes, O. Chubykalo-Fesenko, H. Kachkachi, D. A. Garanin, R. Evans, R. W. Chantrell, Phys. Rev. B 2007, 76, 064416;
b) V. Russier, C. de-Montferrand, Y. Lalatonne, L. Motte, J. Appl. Phys. 2013, 114, 143904;
c) K. L. Pisane, S. Singh, M. S. Seehra, Appl. Phys. Lett. 2017, 110, 222409;
d) W. Baaziz, B. P. Pichon, C. Lefevre, C. Ulhaq-Bouillet, J.-M. Greneche, M. Toumi, T. Mhiri, S. Bégin-Colin, J. Phys. Chem. C 2013, 117, 11436;
e) A. Mitra, J. Mohapatra, S. S. Meena, C. V. Tomy, M. Aslam, J. Phys. Chem. C 2014, 118, 19356;
f) B. Gross, S. Philipp, E. Josten, J. Leliaert, E. Wetterskog, L. Bergström, M. Poggio, Phys. Rev. B 2021, 103, 014402.
a) M. Blanco-Mantecón, K. O'Grady, J. Magn. Magn. Mater. 2006, 296, 124;
b) G. Barrera, P. Allia, P. Tiberto, Nanoscale 2021, 13, 4103.
J. Brunner, I. A. Baburin, S. Sturm, K. Kvashnina, A. Rossberg, T. Pietsch, S. Andreev, E. Sturm, H. Cölfen, Adv. Mater. Interfaces 2017, 4, 1600431.
a) I. Lisiecki, D. Parker, C. Salzemann, M. P. Pileni, Chem. Mater. 2007, 19, 4030;
b) J. Chen, A. Dong, J. Cai, X. Ye, Y. Kang, J. M. Kikkawa, C. B. Murray, Nano Lett. 2010, 10, 5103.
A. Guinier, G. Fournet, Small-Angle Scattering of X-rays, John Wiley & Sons, New York 1955.
a) B. Gurun, Y. S. Thio, D. G. Bucknall, Rev. Sci. Instrum. 2009, 80, 123906;
b) J. Baldrian, M. Steinhart, P. Vlček, M. Horký, P. Laggner, H. Amenitsch, S. Bernstorff, J. Macromol. Sci., Part B: Phys. 2002, 41, 1023;
c) D. Pontoni, J. Bolze, N. Dingenouts, T. Narayanan, M. Ballauff, J. Phys. Chem. B 2003, 107, 5123.
a) T. Beuvier, E. A. C. Panduro, P. Kwaśniewski, S. Marre, C. Lecoutre, Y. Garrabos, C. Aymonier, B. Calvignac, A. Gibaud, Lab Chip 2015, 15, 2002;
b) T. Beuvier, I. Probert, L. Beaufort, B. Suchéras-Marx, Y. Chushkin, F. Zontone, A. Gibaud, Nat. Commun. 2019, 10, 751.
J. Daniels, J. Appl. Crystallogr. 2008, 41, 1109.
S. Nikitenko, A. M. Beale, A. M. J. van der Eerden, S. D. M. Jacques, O. Leynaud, M. G. O'Brien, D. Detollenaere, R. Kaptein, B. M. Weckhuysen, W. Bras, J. Synchrotron Radiat. 2008, 15, 632.
a) J. Schlotheuber né Brunner, B. Maier, S. L. J. Thomä, F. Kirner, I. A. Baburin, D. Lapkin, R. Rosenberg, S. Sturm, D. Assalauova, J. Carnis, Y. Y. Kim, Z. Ren, F. Westermeier, S. Theiss, H. Borrmann, S. Polarz, A. Eychmüller, A. Lubk, I. A. Vartanyants, H. Cölfen, M. Zobel, E. V. Sturm, Chem. Mater. 2021, 33, 9119.
b) J. J. Schlotheuber née Brunner, B. Maier, F. Kirner, S. Sturm, H. Cölfen, E. V. Sturm, Cryst. Growth Des. 2021, 21, 5490.
J. Brunner, B. Maier, R. Rosenberg, S. Sturm, H. Cölfen, E. V. Sturm, Chem. - Eur. J. 2020, 26,15242.
Z. Nedelkoski, D. Kepaptsoglou, L. Lari, T. Wen, R. A. Booth, S. D. Oberdick, P. L. Galindo, Q. M. Ramasse, R. F. L. Evans, S. Majetich, V. K. Lazarov, Sci. Rep. 2017, 7, 45997.
T. Kohler, A. Feoktystov, O. Petracic, N. Nandakumaran, A. Cervellino, T. Bruckel, J. Appl. Crystallogr. 2021, 54, 1719.
V. Chlan, J. Żukrowski, A. Bosak, Z. Kąkol, A. Kozłowski, Z. Tarnawski, R. Řezníček, H. Štěpánková, P. Novák, I. Biało, J. M. Honig, Phys. Rev. B 2018, 98, 125138.
T. Welberry, J. Appl. Cryst. 1986, 19, 382.
I. J. Bruvera, P. M. Zélis, M. P. Calatayud, G. F. Goya, F. H. Sánchez, J. Appl. Phys. 2015, 118, 184304.
H. Mamiya, H. Fukumoto, J. L. C. Huaman, K. Suzuki, H. Miyamura, J. Balachandran, ACS Nano 2020, 14, 8421.
J. Dai, J.-Q. Wang, C. Sangregorio, J. Fang, E. Carpenter, J. Tang, J. Appl. Phys. 2000, 87, 7397.
J. Schindelin, I. Arganda-Carreras, E. Frise, V. Kaynig, M. Longair, T. Pietzsch, S. Preibisch, C. Rueden, S. Saalfeld, B. Schmid, J.-Y. Tinevez, D. J. White, V. Hartenstein, K. Eliceiri, P. Tomancak, A. Cardona, Nat. Methods 2012, 9, 676.
I. Arganda-Carreras, V. Kaynig, C. Rueden, K. W. Eliceiri, J. Schindelin, A. Cardona, H. S. Seung, Bioinformatics 2017, 33, 2424.
CrysAlisPRO, Rigaku Oxford Diffraction.
A. Girard, T. Nguyen-Thanh, S. M. Souliou, M. Stekiel, W. Morgenroth, L. Paolasini, A. Minelli, D. Gambetti, B. Winkler, A. Bosak, J. Synchrotron Radiat. 2019, 26, 272.