Superchaotropic Nano-ion Binding as a Gelation Motif in Cellulose Ether Solutions.

Cellulose Chaotropic Effect Hydrogel Polyoxometalate Superchaotropic

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
16 01 2023
Historique:
received: 12 07 2022
pubmed: 9 11 2022
medline: 12 1 2023
entrez: 8 11 2022
Statut: ppublish

Résumé

Nanometer-sized anions (nano-ions) like polyoxometalates and boron clusters exhibit so-called superchaotropic behavior, which describes their strong binding to hydrated non-ionic matter in water. We show here that nano-ions, at millimolar concentrations, dramatically enhance the viscosity and induce gelation of aqueous solutions of non-ionic cellulose ethers (CEs), a class of widely utilized polymers known for their thickening and gel-forming ability. These phenomena arise from an interplay of attractive forces and repulsive electrostatic forces between CE-chains upon nano-ion binding. The attractive forces manifest themselves as aggregation of CE-chains into a physically crosslinked polymer network (gel). In turn, the electrostatic repulsions hamper the viscosity increase and gelation. Superchaotropic nano-ion binding emerges as a novel and general physical crosslinking motif for CE-solutions and exceeds by far the conventional thickening effects of classical salts and ionic surfactants.

Identifiants

pubmed: 36346946
doi: 10.1002/anie.202210208
pmc: PMC10107358
doi:

Substances chimiques

Cellulose 9004-34-6
Ether 0F5N573A2Y
Polymers 0
Water 059QF0KO0R
Ethyl Ethers 0
Ethers 0
Solutions 0

Types de publication

Journal Article Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202210208

Informations de copyright

© 2022 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Max Hohenschutz (M)

RWTH Aachen University, Institute of Physical Chemistry, Landoltweg 2, 52074, Aachen, Germany.

Pierre Bauduin (P)

Institut de Chimie Séparative de Marcoule, ICSM, CEA, CNRS, ENSCM, Univ Montpellier, Marcoule, France.

Carlos G Lopez (CG)

RWTH Aachen University, Institute of Physical Chemistry, Landoltweg 2, 52074, Aachen, Germany.

Beate Förster (B)

Forschungszentrum Jülich GmbH, Ernst Ruska-Centrum für Mikroskopie und Spektroskopie mit Elektronen (ER-C-1), 52425, Jülich, Germany.

Walter Richtering (W)

RWTH Aachen University, Institute of Physical Chemistry, Landoltweg 2, 52074, Aachen, Germany.
DWI-Leibniz-Institute for Interactive Materials e.V., RWTH-Aachen University, Forckenbeckstraße 50, 52074, Aachen, Germany.

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Classifications MeSH