A Combined Raman Spectroscopy and Atomic Force Microscopy System for In Situ and Real-Time Measures in Electrochemical Cells.
HOPG intercalation
Raman spectroscopy
in situ AFM
solid–liquid interface
Journal
Materials (Basel, Switzerland)
ISSN: 1996-1944
Titre abrégé: Materials (Basel)
Pays: Switzerland
ID NLM: 101555929
Informations de publication
Date de publication:
10 Mar 2023
10 Mar 2023
Historique:
received:
20
01
2023
revised:
07
03
2023
accepted:
08
03
2023
medline:
30
3
2023
entrez:
29
3
2023
pubmed:
30
3
2023
Statut:
epublish
Résumé
An innovative and versatile set-up for in situ and real time measures in an electrochemical cell is described. An original coupling between micro-Raman spectroscopy and atomic force microscopy enables one to collect data on opaque electrodes. This system allows for the correlation of topographic images with chemical maps during the charge exchange occurring in oxidation/reduction processes. The proposed set-up plays a crucial role when reactions, both reversible and non-reversible, are studied step by step during electrochemical reactions and/or when local chemical analysis is required.
Identifiants
pubmed: 36984119
pii: ma16062239
doi: 10.3390/ma16062239
pmc: PMC10051831
pii:
doi:
Types de publication
Journal Article
Langues
eng
Références
Science. 1988 Oct 14;242(4876):209-16
pubmed: 3051380
Rev Sci Instrum. 2022 Jul 1;93(7):073707
pubmed: 35922332
Science. 1986 Apr 11;232(4747):211-3
pubmed: 17780805
Phys Chem Chem Phys. 2017 May 31;19(21):13855-13859
pubmed: 28513671
Anal Chem. 2017 Sep 5;89(17):8974-8980
pubmed: 28799750
Phys Rev Lett. 1986 Mar 3;56(9):930-933
pubmed: 10033323
Appl Opt. 2020 Sep 20;59(27):8175-8181
pubmed: 32976398
Appl Spectrosc. 2012 Dec;66(12):1365-84
pubmed: 23231899