Modular 3D-printed fluorometer/photometer for determination of iron(ii), caffeine, and ciprofloxacin in pharmaceutical samples.


Journal

RSC advances
ISSN: 2046-2069
Titre abrégé: RSC Adv
Pays: England
ID NLM: 101581657

Informations de publication

Date de publication:
17 Apr 2023
Historique:
received: 24 02 2023
accepted: 09 04 2023
medline: 20 4 2023
pubmed: 20 4 2023
entrez: 20 04 2023
Statut: epublish

Résumé

The demand for the development of portable and low-cost analytical devices has encouraged studies employing additive manufacturing techniques, such as 3D-printing. This method can be used to produce components such as printed electrodes, photometers, and fluorometers for low-cost systems that provide advantages including low sample volume, reduced chemical waste, and easy coupling with LED-based optics and other instrumental devices. In the present work, a modular 3D-printed fluorometer/photometer was designed and applied for the determination of caffeine (CAF), ciprofloxacin (CIP), and Fe(ii) in pharmaceutical samples. All the plastic parts were printed separately by a 3D printer, using Tritan as the plastic material (black color). The final size of the modular 3D-printed device was 12 × 8 cm. The radiation sources were light-emitting diodes (LEDs), while a light dependent resistor (LDR) was used as a photodetector. The analytical curves obtained for the device were:

Identifiants

pubmed: 37077256
doi: 10.1039/d3ra01281f
pii: d3ra01281f
pmc: PMC10108832
doi:

Types de publication

Journal Article

Langues

eng

Pagination

12050-12058

Informations de copyright

This journal is © The Royal Society of Chemistry.

Déclaration de conflit d'intérêts

There are no conflicts to declare.

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Auteurs

Rafaela Silva Lamarca (RS)

Department of Analytical Chemistry, Physical Chemistry and Inorganic Chemistry, National Institute for Alternative Technologies of Detection, Toxicological Evaluation and Removal of Micropollutants and Radioactives (INCT-DATREM), Institute of Chemistry, São Paulo State University (UNESP) Araraquara São Paulo 14800-060 Brazil paulo.clairmont@unesp.br.

João Pedro Silva (JP)

Department of Analytical Chemistry, Physical Chemistry and Inorganic Chemistry, National Institute for Alternative Technologies of Detection, Toxicological Evaluation and Removal of Micropollutants and Radioactives (INCT-DATREM), Institute of Chemistry, São Paulo State University (UNESP) Araraquara São Paulo 14800-060 Brazil paulo.clairmont@unesp.br.

João Paulo Varoni Dos Santos (JP)

Department of Analytical Chemistry, Physical Chemistry and Inorganic Chemistry, National Institute for Alternative Technologies of Detection, Toxicological Evaluation and Removal of Micropollutants and Radioactives (INCT-DATREM), Institute of Chemistry, São Paulo State University (UNESP) Araraquara São Paulo 14800-060 Brazil paulo.clairmont@unesp.br.

Saidy Cristina Ayala-Durán (SC)

Department of Analytical Chemistry, Physical Chemistry and Inorganic Chemistry, National Institute for Alternative Technologies of Detection, Toxicological Evaluation and Removal of Micropollutants and Radioactives (INCT-DATREM), Institute of Chemistry, São Paulo State University (UNESP) Araraquara São Paulo 14800-060 Brazil paulo.clairmont@unesp.br.

Paulo Clairmont Feitosa de Lima Gomes (PCF)

Department of Analytical Chemistry, Physical Chemistry and Inorganic Chemistry, National Institute for Alternative Technologies of Detection, Toxicological Evaluation and Removal of Micropollutants and Radioactives (INCT-DATREM), Institute of Chemistry, São Paulo State University (UNESP) Araraquara São Paulo 14800-060 Brazil paulo.clairmont@unesp.br.

Classifications MeSH