Analytical quality-by-design approach for development and validation of HPLC method for the simultaneous estimation of omarigliptin, metformin, and ezetimibe: application to human plasma and dosage forms.

Ezetimibe HPLC Metformin Omarigliptin Quality by design

Journal

BMC chemistry
ISSN: 2661-801X
Titre abrégé: BMC Chem
Pays: Switzerland
ID NLM: 101741142

Informations de publication

Date de publication:
05 May 2023
Historique:
received: 07 01 2023
accepted: 14 04 2023
medline: 6 5 2023
pubmed: 6 5 2023
entrez: 5 5 2023
Statut: epublish

Résumé

A simple, selective, and sensitive RP-HPLC method was proposed for the simultaneous determination of two co-administered antidiabetic drugs (omarigliptin and metformin) with an anti-hyperlipidemic drug (ezetimibe) in a medicinally-recommended ratio of 2.5:50:1, respectively. The proposed procedure was optimized by adopting a quality-by-design approach. The influence of different factors on chromatographic responses was optimized by applying the two-level full factorial design (2

Identifiants

pubmed: 37147652
doi: 10.1186/s13065-023-00955-w
pii: 10.1186/s13065-023-00955-w
pmc: PMC10163694
doi:

Types de publication

Journal Article

Langues

eng

Pagination

45

Informations de copyright

© 2023. The Author(s).

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Auteurs

Galal Magdy (G)

Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Kafrelsheikh University, P.O. Box 33511, Kafrelsheikh, Egypt. galal_magdy@pharm.kfs.edu.eg.

Amira A Al-Enna (AA)

Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Kafrelsheikh University, P.O. Box 33511, Kafrelsheikh, Egypt.

Fathalla Belal (F)

Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Mansoura University, P.O. Box 35516, Mansoura, Egypt.

Ramadan A El-Domany (RA)

Microbiology and Immunology Department, Faculty of Pharmacy, Kafrelsheikh University, P.O. Box 33511, Kafrelsheikh, Egypt.

Ahmed M Abdel-Megied (AM)

Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Kafrelsheikh University, P.O. Box 33511, Kafrelsheikh, Egypt.
Department of Pharmaceutical Sciences, School of Pharmacy, Notre Dame of Maryland University, Baltimore, MD, 21210, USA.

Classifications MeSH