Development and validation of an LC-MS/MS method for quantification of favipiravir in human plasma.


Journal

Journal of pharmaceutical and biomedical analysis
ISSN: 1873-264X
Titre abrégé: J Pharm Biomed Anal
Pays: England
ID NLM: 8309336

Informations de publication

Date de publication:
05 Sep 2023
Historique:
received: 24 03 2023
revised: 21 04 2023
accepted: 30 04 2023
medline: 12 6 2023
pubmed: 7 5 2023
entrez: 6 5 2023
Statut: ppublish

Résumé

Favipiravir (FVP) is a broad-spectrum antiviral that selectively inhibits viral RNA-dependent RNA polymerase, first trialled for the treatment of influenza infection. It has been shown to be effective against a number of RNA virus families including arenaviruses, flaviviruses and enteroviruses. Most recently, FVP has been investigated as a potential therapeutic for severe acute respiratory syndrome coronavirus 2 infection. A liquid chromatography tandem mass spectrometry method for the quantification of FVP in human plasma has been developed and validated for use in clinical trials investigating favipiravir as treatment for coronavirus disease-2019. Samples were extracted by protein precipitation using acetonitrile, using

Identifiants

pubmed: 37148698
pii: S0731-7085(23)00205-4
doi: 10.1016/j.jpba.2023.115436
pii:
doi:

Substances chimiques

formic acid 0YIW783RG1
favipiravir EW5GL2X7E0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

115436

Subventions

Organisme : Medical Research Council
ID : MR/V028391/1
Pays : United Kingdom

Informations de copyright

Copyright © 2023 The Authors. Published by Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of Competing Interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Elizabeth Challenger (E)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK. Electronic address: echall@liverpool.ac.uk.

Sujan Dilly Penchala (SD)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK.

Colin Hale (C)

Liverpool University Hospitals NHS Foundation Trust, Prescot Street, Liverpool L7 8XP, UK.

Richard Fitzgerald (R)

Liverpool University Hospitals NHS Foundation Trust, Prescot Street, Liverpool L7 8XP, UK.

Lauren Walker (L)

Liverpool University Hospitals NHS Foundation Trust, Prescot Street, Liverpool L7 8XP, UK.

Helen Reynolds (H)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK.

Justin Chiong (J)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK.

Tom Fletcher (T)

Liverpool School of Tropical Medicine, Pembroke Place, Liverpool L3 5QA, UK.

Saye Khoo (S)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK; Liverpool University Hospitals NHS Foundation Trust, Prescot Street, Liverpool L7 8XP, UK.

Laura Else (L)

Department of Molecular and Clinical Pharmacology, University of Liverpool, Liverpool L7 8TX, UK.

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Classifications MeSH