Unraveling the Complex Solid-State Phase Transition Behavior of 1-Iodoadamantane, a Material for Which Ostensibly Identical Crystals Undergo Different Transformation Pathways.
Journal
Crystal growth & design
ISSN: 1528-7483
Titre abrégé: Cryst Growth Des
Pays: United States
ID NLM: 101261892
Informations de publication
Date de publication:
03 May 2023
03 May 2023
Historique:
received:
26
02
2023
revised:
20
03
2023
medline:
9
5
2023
pubmed:
9
5
2023
entrez:
9
5
2023
Statut:
epublish
Résumé
Phase transitions in crystalline molecular solids have important implications in the fundamental understanding of materials properties and in the development of materials applications. Herein, we report the solid-state phase transition behavior of 1-iodoadamantane (1-IA) investigated using a multi-technique strategy [synchrotron powder X-ray diffraction (XRD), single-crystal XRD, solid-state NMR, and differential scanning calorimetry (DSC)], which reveals complex phase transition behavior on cooling from ambient temperature to ca. 123 K and on subsequent heating to the melting temperature (348 K). Starting from the known phase of 1-IA at ambient temperature (phase
Identifiants
pubmed: 37159655
doi: 10.1021/acs.cgd.3c00223
pmc: PMC10161194
doi:
Types de publication
Journal Article
Langues
eng
Pagination
3820-3833Informations de copyright
© 2023 The Authors. Published by American Chemical Society.
Déclaration de conflit d'intérêts
The authors declare no competing financial interest.
Références
Biopolymers. 2014 Mar;101(3):246-56
pubmed: 23784805
Phys Chem Chem Phys. 2016 Apr 28;18(16):10924-30
pubmed: 27040739
Angew Chem Int Ed Engl. 2003 Jul 7;42(26):2982-5
pubmed: 12851948
Phys Chem Chem Phys. 2021 Oct 20;23(40):23274-23279
pubmed: 34632470
Rev Sci Instrum. 2009 Jul;80(7):075107
pubmed: 19655981
ACS Cent Sci. 2019 Aug 28;5(8):1315-1329
pubmed: 31482114
Acta Crystallogr A. 2008 Jan;64(Pt 1):149-60
pubmed: 18156680
Acta Crystallogr C Struct Chem. 2015 Jan;71(Pt 1):3-8
pubmed: 25567568
Angew Chem Int Ed Engl. 2018 Dec 10;57(50):16313-16317
pubmed: 30325568
J Phys Chem B. 2005 Dec 15;109(49):23342-50
pubmed: 16375305
Phys Chem Chem Phys. 2017 Aug 2;19(30):20259-20266
pubmed: 28726892
J Phys Chem A. 2013 Aug 22;117(33):7855-62
pubmed: 23879450
Ultramicroscopy. 2007 Jun-Jul;107(6-7):507-13
pubmed: 17234347
Angew Chem Int Ed Engl. 2020 Dec 7;59(50):22638-22644
pubmed: 32885575
J Chem Phys. 2010 Apr 28;132(16):164516
pubmed: 20441297
Biopolymers. 2005 Mar;77(4):230-45
pubmed: 15674975
Acta Crystallogr Sect E Struct Rep Online. 2008 Dec 13;65(Pt 1):o101
pubmed: 21581565
Chem Commun (Camb). 2011 Apr 7;47(13):3760-2
pubmed: 21293806
Science. 2017 Jan 13;355(6321):166-169
pubmed: 28082587
Science. 2014 May 30;344(6187):1013-6
pubmed: 24876494
IUCrJ. 2015 Jan 01;2(Pt 1):126-36
pubmed: 25610633