A Rapid and Sensitive Stability-Indicating Eco-Friendly HPTLC Assay for Fluorescence Detection of Ergotamine.

Chromatography, Thin Layer / methods Chromatography, High Pressure Liquid / methods Reproducibility of Results Tablets Ergotamines
AGREE eco-friendly HPTLC ergotamine fluorescence detection stability indicating validation

Journal

Molecules (Basel, Switzerland)
ISSN: 1420-3049
Titre abrégé: Molecules
Pays: Switzerland
ID NLM: 100964009

Informations de publication

Date de publication:
29 Jun 2023
Historique:
received: 18 06 2023
revised: 26 06 2023
accepted: 27 06 2023
medline: 17 7 2023
pubmed: 14 7 2023
entrez: 14 7 2023
Statut: epublish

Résumé

Eco-friendly liquid chromatographic methods for measuring ergotamine (EGT) are scant in the published database. Accordingly, the goal of the current study was to develop a high-performance thin-layer chromatography (HPTLC) method for fluorescence detection of EGT in commercially available tablets. This approach was based on the application of ethyl alcohol-water (80:20

Identifiants

DOI: 10.3390/molecules28135101 PMID: 37446763 PMC: PMC10343250
pubmed: 37446763
pii: molecules28135101
doi: 10.3390/molecules28135101
pmc: PMC10343250
pii:
doi:

Substances chimiques

Tablets 0
Ergotamines 0

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Deputyship for Research & Innovation, Ministry of Education
ID : IFKSUOR3-066

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Auteurs

Faiyaz Shakeel (F)

Department of Pharmaceutics, College of Pharmacy, King Saud University, Riyadh 11451, Saudi Arabia.
ORCID: 0000-0002-6109-0885

Prawez Alam (P)

Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, Al-Kharj 11942, Saudi Arabia.
ORCID: 0000-0002-7632-3426

Mohammed H Alqarni (MH)

Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, Al-Kharj 11942, Saudi Arabia.
ORCID: 0000-0002-7061-9111

Nazrul Haq (N)

Department of Pharmaceutics, College of Pharmacy, King Saud University, Riyadh 11451, Saudi Arabia.
ORCID: 0000-0003-0666-808X

Fatma M Abdel Bar (FMA)

Department of Pharmacognosy, College of Pharmacy, Prince Sattam Bin Abdulaziz University, Al-Kharj 11942, Saudi Arabia.
ORCID: 0000-0003-0823-4015

Muzaffar Iqbal (M)

Department of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, Riyadh 11451, Saudi Arabia.
ORCID: 0000-0001-5821-5600

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Classifications MeSH

questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie sur couche mince › A Rapid and Sensitive Stability-Indicating...
questionsmedicales.fr › Techniques d'investigation › Techniques de chimie analytique › Chromatographie › Chromatographie en phase liquide › Chromatographie en phase liquide à haute performance › A Rapid and Sensitive Stability-Indicating...
questionsmedicales.fr › Environnement et santé publique › Santé publique › Méthodes épidémiologiques › Méthodologie en recherche épidémiologique › Reproductibilité des résultats › A Rapid and Sensitive Stability-Indicating...
questionsmedicales.fr › Préparations pharmaceutiques › Comprimés › A Rapid and Sensitive Stability-Indicating...
questionsmedicales.fr › Composés hétérocycliques › Composés hétérocycliques à cycles fusionnés › Composés hétérocycliques avec 4 noyaux ou plus › Ergotamines › A Rapid and Sensitive Stability-Indicating...