Determination of scopolamine and butylscopolamine in beverages, urine and Buscopan® tablets samples using electrophoresis microchip with integrated contactless conductivity detection.

Electrochemical detection Forensic chemistry Microfluidics Predatory drugs Tropane alkaloids

Journal

Talanta
ISSN: 1873-3573
Titre abrégé: Talanta
Pays: Netherlands
ID NLM: 2984816R

Informations de publication

Date de publication:
01 Jan 2024
Historique:
received: 26 03 2023
revised: 16 06 2023
accepted: 15 07 2023
medline: 20 9 2023
pubmed: 24 7 2023
entrez: 24 7 2023
Statut: ppublish

Résumé

The number of cases in which scopolamine (SCO) was used for both recreational and predatory purposes has increased dramatically in recent decades. Linked to this, there is a concern about obtaining SCO through thermal degradation of butylscopolamine (BSCO) - an active ingredient of Buscopan® - a drug sold without a medical prescription. In this study, mixtures containing SCO and BSCO were separated and detected on a microchip electrophoresis (ME) device with integrated capacitively coupled contactless conductivity detection (C

Identifiants

pubmed: 37487267
pii: S0039-9140(23)00711-7
doi: 10.1016/j.talanta.2023.124960
pii:
doi:

Substances chimiques

Butylscopolammonium Bromide 2Z3E1OF81V
Scopolamine DL48G20X8X
Tablets 0
Butyric Acid 107-92-6

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

124960

Informations de copyright

Copyright © 2023 Elsevier B.V. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of competing interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Hellen I Santos (HI)

Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.

Kemilly M P Pinheiro (KMP)

Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil.

Eduardo M Richter (EM)

Instituto de Química, Universidade Federal de Uberlândia, 38408-100, Uberlândia, MG, Brazil; Instituto Nacional de Ciência e Tecnologia de Bioanalítica, 13084-971, Campinas, SP, Brazil.

Wendell K T Coltro (WKT)

Instituto de Química, Universidade Federal de Goiás, 74690-900, Goiânia, GO, Brazil; Instituto Nacional de Ciência e Tecnologia de Bioanalítica, 13084-971, Campinas, SP, Brazil. Electronic address: wendell@ufg.br.

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Classifications MeSH