Chemo-Enzymatic Fluorescence Labeling Of Genomic DNA For Simultaneous Detection Of Global 5-Methylcytosine And 5-Hydroxymethylcytosine.

5-hydroxymethylcytosine DNA methylation DNA methyltransferase epigenetic biomarker fluorescence

Journal

Chembiochem : a European journal of chemical biology
ISSN: 1439-7633
Titre abrégé: Chembiochem
Pays: Germany
ID NLM: 100937360

Informations de publication

Date de publication:
17 10 2023
Historique:
revised: 05 07 2023
received: 29 05 2023
medline: 23 10 2023
pubmed: 31 7 2023
entrez: 30 7 2023
Statut: ppublish

Résumé

5-Methylcytosine and 5-hydroxymethylcytosine are epigenetic modifications involved in gene regulation and cancer. We present a new, simple, and high-throughput platform for multi-color epigenetic analysis. The novelty of our approach is the ability to multiplex methylation and de-methylation signals in the same assay. We utilize an engineered methyltransferase enzyme that recognizes and labels all unmodified CpG sites with a fluorescent cofactor. In combination with the already established labeling of the de-methylation mark 5-hydroxymethylcytosine via enzymatic glycosylation, we obtained a robust platform for simultaneous epigenetic analysis of these marks. We assessed the global epigenetic levels in multiple samples of colorectal cancer and observed a 3.5-fold reduction in 5hmC levels but no change in DNA methylation levels between sick and healthy individuals. We also measured epigenetic modifications in chronic lymphocytic leukemia and observed a decrease in both modification levels (5-hydroxymethylcytosine: whole blood 30 %; peripheral blood mononuclear cells (PBMCs) 40 %. 5-methylcytosine: whole blood 53 %; PBMCs 48 %). Our findings propose using a simple blood test as a viable method for analysis, simplifying sample handling in diagnostics. Importantly, our results highlight the assay's potential for epigenetic evaluation of clinical samples, benefiting research and patient management.

Identifiants

pubmed: 37518671
doi: 10.1002/cbic.202300400
doi:

Substances chimiques

5-hydroxymethylcytosine 1123-95-1
5-Methylcytosine 6R795CQT4H
DNA 9007-49-2

Types de publication

Journal Article Research Support, N.I.H., Extramural Research Support, Non-U.S. Gov't

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202300400

Subventions

Organisme : European Research Council
ID : 817811
Pays : International
Organisme : NHGRI NIH HHS
ID : R01HG009190
Pays : United States

Informations de copyright

© 2023 The Authors. ChemBioChem published by Wiley-VCH GmbH.

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Auteurs

Sigal Avraham (S)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Leonie Schütz (L)

Institute of Organic Chemistry, RWTH Aachen University, 52056, Aachen, Germany.

Larissa Käver (L)

Institute of Organic Chemistry, RWTH Aachen University, 52056, Aachen, Germany.

Andreas Dankers (A)

Institute of Organic Chemistry, RWTH Aachen University, 52056, Aachen, Germany.

Sapir Margalit (S)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.

Yael Michaeli (Y)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Shahar Zirkin (S)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Dmitry Torchinsky (D)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Noa Gilat (N)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Omer Bahr (O)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Gil Nifker (G)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

Maya Koren-Michowitz (M)

Hematology department, Shamir Medical Center, Be'er Ya'akov, 70300, Israel.

Elmar Weinhold (E)

Institute of Organic Chemistry, RWTH Aachen University, 52056, Aachen, Germany.

Yuval Ebenstein (Y)

Department of Chemistry, Raymond and Beverly SacklerFaculty of Exact Sciences, Department of Biomedical Engineering, Tel Aviv University Tel Aviv-Yafo, 6997801, Tel Aviv, Israel.
School of Chemistry,Ramat Aviv, Tel Aviv University, Tel Aviv, 6997801, Israel.

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