In Situ Ultra-Small- and Small-Angle X-ray Scattering Study of ZnO Nanoparticle Formation and Growth through Chemical Bath Deposition in the Presence of Polyvinylpyrrolidone.
PVP
SAXS
USAXS
ZnO
chemical bath deposition
kinetics
particle formation
polyvinylpyrrolidone
Journal
Nanomaterials (Basel, Switzerland)
ISSN: 2079-4991
Titre abrégé: Nanomaterials (Basel)
Pays: Switzerland
ID NLM: 101610216
Informations de publication
Date de publication:
26 Jul 2023
26 Jul 2023
Historique:
received:
07
07
2023
revised:
20
07
2023
accepted:
21
07
2023
medline:
12
8
2023
pubmed:
12
8
2023
entrez:
12
8
2023
Statut:
epublish
Résumé
ZnO inverse opals combine the outstanding properties of the semiconductor ZnO with the high surface area of the open-porous framework, making them valuable photonic and catalysis support materials. One route to produce inverse opals is to mineralize the voids of close-packed polymer nanoparticle templates by chemical bath deposition (CBD) using a ZnO precursor solution, followed by template removal. To ensure synthesis control, the formation and growth of ZnO nanoparticles in a precursor solution containing the organic additive polyvinylpyrrolidone (PVP) was investigated by in situ ultra-small- and small-angle X-ray scattering (USAXS/SAXS). Before that, we studied the precursor solution by in-house SAXS at
Identifiants
pubmed: 37570497
pii: nano13152180
doi: 10.3390/nano13152180
pmc: PMC10421471
pii:
doi:
Types de publication
Journal Article
Langues
eng
Subventions
Organisme : Deutsche Forschungsgemeinschaft
ID : 358283783
Références
Polymers (Basel). 2018 Oct 11;10(10):
pubmed: 30961054
Science. 1998 Aug 14;281(5379):969-71
pubmed: 9703506
J Colloid Interface Sci. 2005 Aug 1;288(1):313-6
pubmed: 15927594
Adv Mater. 2011 Nov 9;23(42):4918-22
pubmed: 21959928
Langmuir. 2010 May 4;26(9):6494-502
pubmed: 20121159
Nanotechnology. 2009 Sep 9;20(36):365302
pubmed: 19687540
Langmuir. 2015 Feb 3;31(4):1421-8
pubmed: 25587750
Chemistry. 2011 Mar 1;17(10):2923-30
pubmed: 21294196
Chem Soc Rev. 2011 Feb;40(2):696-753
pubmed: 21229132
Langmuir. 2006 Jul 18;22(15):6539-48
pubmed: 16830995
J Phys Chem A. 2016 May 19;120(19):3253-9
pubmed: 26963367
J Mater Sci. 2020;55(7):3005-3021
pubmed: 32431364
Chem Rev. 2010 Mar 10;110(3):1348-85
pubmed: 20108978
Langmuir. 2019 Sep 10;35(36):11702-11709
pubmed: 31403801
J Am Chem Soc. 2021 May 5;143(17):6305-6322
pubmed: 33826324
Langmuir. 2015 Apr 7;31(13):3897-903
pubmed: 25768914
Sci Rep. 2016 May 23;6:26518
pubmed: 27212583
J Appl Crystallogr. 2018;51 Pt 3:
pubmed: 30996401
Chem Rev. 2008 Sep;108(9):3893-957
pubmed: 18720998
Chemphyschem. 2005 Apr;6(4):690-6
pubmed: 15881585
Biotechnol Bioeng. 2012 Jan;109(1):16-30
pubmed: 21915854
Dalton Trans. 2015 Nov 7;44(41):17883-905
pubmed: 26434727
J Appl Crystallogr. 2018 Oct 11;51(Pt 6):1511-1524
pubmed: 30546286
Nanomaterials (Basel). 2021 Jan 14;11(1):
pubmed: 33466679
ACS Omega. 2020 Apr 26;5(17):9985-9990
pubmed: 32391486
J Am Chem Soc. 2005 Jun 8;127(22):8179-84
pubmed: 15926847
J Colloid Interface Sci. 2008 Jan 15;317(2):351-74
pubmed: 18028940
Chem Rev. 2008 Nov;108(11):4332-432
pubmed: 19006397
ACS Macro Lett. 2016 Apr 19;5(4):523-527
pubmed: 35607227