Multi-directional neutron dark-field imaging with single absorption grating.


Journal

Scientific reports
ISSN: 2045-2322
Titre abrégé: Sci Rep
Pays: England
ID NLM: 101563288

Informations de publication

Date de publication:
15 Sep 2023
Historique:
received: 22 05 2023
accepted: 08 09 2023
medline: 16 9 2023
pubmed: 16 9 2023
entrez: 15 9 2023
Statut: epublish

Résumé

Neutron dark-field imaging is a powerful technique for investigating the microstructural properties of materials through high-resolution full-field mapping of small-angle scattering. However, conventional neutron dark-field imaging utilizing Talbot-Lau interferometers is limited to probing only one scattering direction at a time. Here, we introduce a novel multi-directional neutron dark-field imaging approach that utilizes a single absorption grating with a two-dimensional pattern to simultaneously probe multiple scattering directions. The method is demonstrated to successfully resolve fiber orientations in a carbon compound material as well as the complex morphology of the transformed martensitic phase in additively manufactured stainless steel dogbone samples after mechanical deformation. The latter results reveal a preferential alignment of transformed domains parallel to the load direction, which is verified by EBSD. The measured real-space correlation functions are in good agreement with those extracted from the EBSD map. Our results demonstrate that multi-directional neutron dark-field imaging is overcoming significant limitations of conventional neutron dark-field imaging in assessing complex heterogeneous anisotropic microstructures and providing quantitative structural information on multiple length scales.

Identifiants

pubmed: 37714939
doi: 10.1038/s41598-023-42310-y
pii: 10.1038/s41598-023-42310-y
pmc: PMC10504250
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

15274

Informations de copyright

© 2023. Springer Nature Limited.

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Auteurs

Matteo Busi (M)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland. matteo.busi@psi.ch.

Jiazhou Shen (J)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland.

Michael Bacak (M)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland.
European Organization for Nuclear Research, CERN, 1211, Geneva, Switzerland.

Marie Christine Zdora (MC)

Institute for Biomedical Engineering, ETH Zürich, 8092, Zurich, Switzerland.
Laboratory for Macromolecules and Bioimaging, Paul Scherrer Institut, 5232, Villigen, Switzerland.

Jan Čapek (J)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland.

Jacopo Valsecchi (J)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland.

Markus Strobl (M)

Laboratory for Neutron Scattering and Imaging, Paul Scherrer Institut, 5232, Villigen, Switzerland. markus.strobl@psi.ch.

Classifications MeSH