High-Affinity Hybridization of Complementary Aromatic Oligoamide Strands in Water.

Aromatic Oligoamide Artificial Hybridization Double Helix Foldamer Self-Assembly

Journal

Angewandte Chemie (International ed. in English)
ISSN: 1521-3773
Titre abrégé: Angew Chem Int Ed Engl
Pays: Germany
ID NLM: 0370543

Informations de publication

Date de publication:
27 Nov 2023
Historique:
received: 10 08 2023
medline: 7 10 2023
pubmed: 7 10 2023
entrez: 7 10 2023
Statut: ppublish

Résumé

We prepared a series of water-soluble aromatic oligoamide sequences all composed of a segment prone to form a single helix and a segment prone to dimerize into a double helix. These sequences exclusively assemble as antiparallel duplexes. The modification of the duplex inner rim by varying the nature of the substituents borne by the aromatic monomers allowed us to identify sequences that can hybridize by combining two chemically different strands, with high affinity and complete selectivity in water. X-ray crystallography confirmed the expected antiparallel configuration of the duplexes whereas NMR spectroscopy and mass spectrometry allowed us to assess precisely the extent of the hybridization. The hybridization kinetics of the aromatic strands was shown to depend on both the nature of the substituents responsible for strand complementarity and the length of the aromatic strand. These results highlight the great potential of aromatic hetero-duplex as a tool to construct non-symmetrical dynamic supramolecular assemblies.

Identifiants

pubmed: 37804233
doi: 10.1002/anie.202311639
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202311639

Informations de copyright

© 2023 The Authors. Angewandte Chemie International Edition published by Wiley-VCH GmbH.

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Auteurs

Victor Koehler (V)

CBMN (UMR 5248) Univ. Bordeaux, CNRS, Bordeaux Institut National Polytechnique, 2 rue Escarpit, 33600, Pessac, France.

Gabrielle Bruschera (G)

CBMN (UMR 5248) Univ. Bordeaux, CNRS, Bordeaux Institut National Polytechnique, 2 rue Escarpit, 33600, Pessac, France.

Eric Merlet (E)

CBMN (UMR 5248) Univ. Bordeaux, CNRS, Bordeaux Institut National Polytechnique, 2 rue Escarpit, 33600, Pessac, France.

Pradeep K Mandal (PK)

Department Pharmazie, Ludwig-Maximilians-Universität München, Butenandtstr. 5-13, 81377, München, Germany.

Estelle Morvan (E)

IECB, UAR3033 Univ. ćBordeaux, CNRS, INSERM, 2 rue Robert Escarpit, 33600, Pessac, France.

Frédéric Rosu (F)

IECB, UAR3033 Univ. ćBordeaux, CNRS, INSERM, 2 rue Robert Escarpit, 33600, Pessac, France.

Céline Douat (C)

Department Pharmazie, Ludwig-Maximilians-Universität München, Butenandtstr. 5-13, 81377, München, Germany.

Lucile Fischer (L)

CBMN (UMR 5248) Univ. Bordeaux, CNRS, Bordeaux Institut National Polytechnique, 2 rue Escarpit, 33600, Pessac, France.

Ivan Huc (I)

Department Pharmazie, Ludwig-Maximilians-Universität München, Butenandtstr. 5-13, 81377, München, Germany.

Yann Ferrand (Y)

CBMN (UMR 5248) Univ. Bordeaux, CNRS, Bordeaux Institut National Polytechnique, 2 rue Escarpit, 33600, Pessac, France.

Classifications MeSH