Oxidation State and Structure of Fe in Nontronite: From Oxidizing to Reducing Conditions.


Journal

ACS earth & space chemistry
ISSN: 2472-3452
Titre abrégé: ACS Earth Space Chem
Pays: United States
ID NLM: 101695267

Informations de publication

Date de publication:
19 Oct 2023
Historique:
received: 19 05 2023
revised: 30 08 2023
accepted: 30 08 2023
medline: 26 10 2023
pubmed: 26 10 2023
entrez: 26 10 2023
Statut: epublish

Résumé

The redox reaction between natural Fe-containing clay minerals and its sorbates is a fundamental process controlling the cycles of many elements such as carbon, nutrients, redox-sensitive metals, and metalloids (e.g., Co, Mn, As, Se), and inorganic as well as organic pollutants in Earth's critical zone. While the structure of natural clay minerals under oxic conditions is well-known, less is known about their behavior under anoxic and reducing conditions, thereby impeding a full understanding of the mechanisms of clay-driven reduction and oxidation (redox) reactions especially under reducing conditions. Here we investigate the structure of a ferruginous natural clay smectite, nontronite, under different redox conditions, and compare several methods for the determination of iron redox states. Iron in nontronite was gradually reduced chemically with the citrate-bicarbonate-dithionite (CBD) method.

Identifiants

pubmed: 37881367
doi: 10.1021/acsearthspacechem.3c00136
pmc: PMC10594735
doi:

Types de publication

Journal Article

Langues

eng

Pagination

1868-1881

Informations de copyright

© 2023 The Authors. Published by American Chemical Society.

Déclaration de conflit d'intérêts

The authors declare no competing financial interest.

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Auteurs

Yanting Qian (Y)

Laboratory for Waste Management, Paul Scherrer Institut, CH-5232 Villigen, Switzerland.
Institute for Geological Sciences, University of Bern, CH-3012 Bern, Switzerland.

Andreas C Scheinost (AC)

The Rossendorf Beamline at the European Synchrotron Radiation Facility (ESRF), Avenue des Martyrs 71, 38043, Grenoble, France.
Helmholtz Zentrum Dresden Rossendorf, Institute of Resource Ecology, Bautzner Landstrasse 400, 01328, Dresden, Germany.

Sylvain Grangeon (S)

BRGM - French Geological Survey, 45060 Orléans, France.

Jean-Marc Greneche (JM)

Institut des Molécules et Matériaux du Mans IMMM UMR CNRS 6283, Le Mans Université, 72085, Le Mans Cedex 9, France.

Alwina Hoving (A)

TNO Geological Survey of The Netherlands, P.O. Box 80015, 3508 TA Utrecht, The Netherlands.

Eric Bourhis (E)

Interfaces, Confinement, Matériaux et Nanostructures (ICMN), CNRS/Université d'Orléans, UMR 7374, 1b rue de la Férollerie, CS 40059, 45071 Orléans, France.

Nicolas Maubec (N)

BRGM - French Geological Survey, 45060 Orléans, France.

Sergey V Churakov (SV)

Laboratory for Waste Management, Paul Scherrer Institut, CH-5232 Villigen, Switzerland.
Institute for Geological Sciences, University of Bern, CH-3012 Bern, Switzerland.

Maria Marques Fernandes (MM)

Laboratory for Waste Management, Paul Scherrer Institut, CH-5232 Villigen, Switzerland.

Classifications MeSH