COF-supported zirconium oxyhydroxide as a versatile heterogeneous catalyst for Knoevenagel condensation and nerve agent hydrolysis.

Interface science Nanoparticles Physical organic chemistry

Journal

iScience
ISSN: 2589-0042
Titre abrégé: iScience
Pays: United States
ID NLM: 101724038

Informations de publication

Date de publication:
17 Nov 2023
Historique:
received: 31 05 2023
revised: 25 06 2023
accepted: 26 09 2023
medline: 9 11 2023
pubmed: 9 11 2023
entrez: 9 11 2023
Statut: epublish

Résumé

A composite of catalytic Lewis acidic zirconium oxyhydroxides (8 wt %) and a covalent organic framework (COF) was synthesized. X-ray diffraction and infrared (IR) spectroscopy reveal that COF's structure is preserved after loading with zirconium oxyhydroxides. Electron microscopy confirms a homogeneous distribution of nano- to sub-micron-sized zirconium clusters in the COF. 3D X-ray tomography captures the micron-sized channels connecting the well-dispersed zirconium clusters on the COF. The crystalline ZrO

Identifiants

pubmed: 37942004
doi: 10.1016/j.isci.2023.108088
pii: S2589-0042(23)02165-X
pmc: PMC10628716
doi:

Types de publication

Journal Article

Langues

eng

Pagination

108088

Informations de copyright

© 2023 The Author(s).

Déclaration de conflit d'intérêts

The authors declare no competing interests.

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Auteurs

Pragalbh Shekhar (P)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Venkata Swaroopa Datta Devulapalli (VS)

Department of Chemistry, Temple University, Philadelphia, PA 19122, USA.

Reshma Reji (R)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Himan Dev Singh (HD)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Aleena Jose (A)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Piyush Singh (P)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Arun Torris (A)

CSIR-NCL, Polymer Science and Engineering (PSE), Pune 411008, India.

Chatakudath P Vinod (CP)

CSIR-NCL Catalysis and Inorganic Chemistry Division, Pune, India.

John A Tokarz (JA)

U.S. Army DEVCOM Chemical Biological Center, Aberdeen Proving Ground, MD 21010, USA.

John J Mahle (JJ)

U.S. Army DEVCOM Chemical Biological Center, Aberdeen Proving Ground, MD 21010, USA.

Gregory W Peterson (GW)

U.S. Army DEVCOM Chemical Biological Center, Aberdeen Proving Ground, MD 21010, USA.

Eric Borguet (E)

Department of Chemistry, Temple University, Philadelphia, PA 19122, USA.

Ramanathan Vaidhyanathan (R)

Department of Chemistry, Indian Institute of Science Education and Research, Pune 411008, India.
Centre for Energy Science, Indian Institute of Science Education and Research, Pune 411008, India.

Classifications MeSH