Carbene-Catalyzed Direct O-Functionalization of Ketone: Atroposelective Access to Non-


Journal

Organic letters
ISSN: 1523-7052
Titre abrégé: Org Lett
Pays: United States
ID NLM: 100890393

Informations de publication

Date de publication:
24 Nov 2023
Historique:
medline: 13 11 2023
pubmed: 13 11 2023
entrez: 13 11 2023
Statut: ppublish

Résumé

Disclosed here is NHC-catalyzed direct intermolecular trapping of the ketone oxygen atom with the acyl azolium intermediate. The overall reaction is a dynamic kinetic resolution process that converts ketone to the corresponding enol ester with well-controlled axial chirality. Our reaction eventually affords non-

Identifiants

pubmed: 37955414
doi: 10.1021/acs.orglett.3c03141
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

8252-8257

Auteurs

Bivas Mondal (B)

School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Hang Chen (H)

School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Rakesh Maiti (R)

School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Hongling Wang (H)

School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Hui Cai (H)

National Key Laboratory of Green Pesticide, Guizhou University, Guiyang, Guizhou 550025, People's Republic of China.

Chengli Mou (C)

School of Pharmacy, Guizhou University of Traditional Chinese Medicine, Guiyang, Guizhou 550025, People's Republic of China.

Lin Hao (L)

School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Huifang Chai (H)

School of Pharmacy, Guizhou University of Traditional Chinese Medicine, Guiyang, Guizhou 550025, People's Republic of China.

Yonggui Robin Chi (YR)

National Key Laboratory of Green Pesticide, Guizhou University, Guiyang, Guizhou 550025, People's Republic of China.
School of Chemistry, Chemical Engineering, and Biotechnology, Nanyang Technological University, 21 Nanyang Link, Singapore 637371, Singapore.

Classifications MeSH