Lycopodium Alkaloids from Phlegmariurus carinatus with Cytotoxic and Neuroprotective Effects.

Huperziaceae Lycopodium alkaloids Phlegmariurus carinatus cytotoxicity neuroprotective activity

Journal

Chemistry & biodiversity
ISSN: 1612-1880
Titre abrégé: Chem Biodivers
Pays: Switzerland
ID NLM: 101197449

Informations de publication

Date de publication:
15 Nov 2023
Historique:
received: 18 09 2023
accepted: 14 11 2023
pubmed: 15 11 2023
medline: 15 11 2023
entrez: 15 11 2023
Statut: aheadofprint

Résumé

One new fawcettimine-type alkaloid, phlecarinadine A (1), and twelve known ones (2-13) were isolated from the whole plant of Phlegmariurus carinatus. Their chemical structures were unambiguously established by extensive spectroscopic analyses, including nuclear magnetic resonance (NMR) spectroscopic and high resolution electrospray ionization mass spectrometry (HR-ESI-MS). The absolute configuration of 1 was elucidated by the electronic circular dichroism (ECD) technique. These compounds were tested for their cytotoxic and neuroprotective activities. None of these compounds revealed cytotoxic activity against five tumor cells. Phlegmariurine B (2) exhibited potential neuroprotective effects against hemin-induced HT22 cell damage, with a 17.76 % increase in cell survival at 10 μM. In further study, 2 can ameliorate hemin-induced neuronal cell death via an anti-apoptotic pathway. These findings suggest that 2 might be a valuable lead compound with neuroprotective activity.

Identifiants

pubmed: 37966166
doi: 10.1002/cbdv.202301449
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e202301449

Subventions

Organisme : National Natural Science Foundation of China
ID : 32260109
Organisme : Science and Technology Plan Project of Jiangxi Provincial Administration of Traditional Chinese Medicine
ID : 2021A325
Organisme : Jiangxi Province Department of Education Science and Technology Research Projects
ID : GJJ211540
Organisme : Jiangxi Province Department of Education Science and Technology Research Projects
ID : GJJ211547

Informations de copyright

© 2023 Wiley-VHCA AG, Zurich, Switzerland.

Références

X. Q. Ma, D. R. Gang, Nat. Prod. Rep. 2004, 21, 752-772.
Y. Hirasawa, J. Kobayashi, H. Morita, Heterocycles 2009, 77, 679-729.
G. Cordell, A. Brossi, The Alkaloids: Chemistry and Pharmacology, Elsevier, Amsterdam, 1994, p. 233.
J. S. Liu, Y. L. Zhu, C. M. Yu, Y. Z. Zhou, Y. Y. Han, F. W. Wu, B. F. Qi, Can. J. Chem. 1986, 64, 837-839.
X. Ma, D. R. Gang, Phytochemistry 2008, 69, 2022-2028.
X. Ma, C. Tan, D. Zhu, D. R. Gang, P. Xiao, J. Ethnopharmacol. 2007, 113, 15-34.
Y. G. Chen, Q. Yang, Y. Zhang, Arab. J. Chem. 2020, 13, 5438-5450.
R. C. Ching, Acta Bot. Yunnan. 1982, 4, 119-128.
Y. G. Wu, L. R. Song, Chinese materia medica, Shanghai Science and Technology Press, Shanghai, 1998, p. 357.
X. C. Zhang, L. B. Zhang, Flora of China, Science Press, Beijing, 2004, p. 53.
F. Liu, Y. C. Liu, W. W. Jiang, J. He, X. D. Wu, L. Y. Peng, J. Xu, X. Cheng, Q. S. Zhao, Nat. Prod. Bioprospect. 2014, 4, 221-225.
W. Thamnarak, W. Thaisaeng, P. Batsomboon, C. Eurtivong, N. Wannarit, S. Ruchirawat, N. Thasana, Phytochemistry 2023, 206, 113553.
C. Wang, X. Z. Yang, G. Mellick, Y. J. Feng, J. Nat. Prod. 2022, 85, 899-909.
W. Thaisaeng, W. Thamnarak, S. Ruchirawat, K. Chainok, N. Thasana, Nat. Prod. Res. 2023, online, https://doi.org/10.1080/14786419.2023.2188587.
Y. Liu, Q. Wang, D. K. Zheng, D. Zhang, Z. Xie, J. W. Hu, X. H. Xie, J. Li, S. P. Jiang, Nat. Prod. Res. 2022, 36, 6006-6011.
J. W. Hu, Q. Wang, L. Liu, Y. M. Hu, M. Xie, D. K. Zheng, Z. Xie, Y. Liu, Phytochemistry 2022, 204, 113457.
K. Ishiuchi, T. Kubota, T. Hoshino, Y. Obara, N. Nakahata, J. Kobayashi, Bioorg. Med. Chem. 2006, 4, 5995-6000.
C. H. Tan, B. D. Wang, S. H. Jiang, D. Y. Zhu, Planta Med. 2002, 68, 188-190.
H. Morita, Y. Hirasawa, J. Kobayashi, J. Nat. Prod. 2005, 68, 1809-1812.
H. Takayama, K. Katakawa, M. Kitajima, K. Yamaguchi, N. Aimi, Chem. Pharm. Bull. 2003, 51, 1163-1169.
J. M. Jiang, D. Xia, X. L. Zhu, D. Zhu, X. W. Yang, K. Pan, Tetrahedron 2022, 114, 132782.
J. S. Liu, M. F. Huang, Phytochemistry 1994, 37, 1759-1761.
X. J. Wang, L. Li, S. S. Yu, S. G. Ma, J. Qu, Y. B. Liu, Y. Li, Y. D. Wang, W. B. Tang, Fitoterapia 2013, 91, 74-81.
C. C. Tan, X. Q. Ma, G. F. Chen, S. H. Jiang, D. Y. Zhu, Chin. Chem. Lett. 2002, 13, 331-332.
C. Peng, X. Gong, Z. Hu, C. Chen, Z. Jiang, PeerJ 2023,11, e15293.
J. Li, L. Q. Li, H. P. Long, J. Liu, Y. P. Jiang, Y. Xue, W. X. Wang, G. S. Tan, Z. C. Gon, J. K. Liu, Phytochemistry 2021, 186, 112729.
Z. X. He, H. F. Song, T. Y. Liu, J. Ma, Z. K. Xing, Y. Y. Yin, L. Liu, Y. N. Zhang, Y. .F. Zhao, H. L. Yu, X. X. He, W. X. Guo, X. J. Zhu, Cereb. Cortex 2019, 29, 2737-2747.

Auteurs

Qiang Wang (Q)

Key Laboratory of Prevention and Treatment of Cardiovascular and Cerebrovascular Diseases, Ministry of Education, Gannan Medical University, Ganzhou, 341000, China.

Dong-Kun Zheng (DK)

National Engineering Research Center for Modernization of Traditional Chinese Medicine-Hakka Medical Resources Branch, College of Pharmacy, Gannan Medical University, Ganzhou, 341000, China.
School of Pharmacy, Nanchang University, Nanchang, People's Republic of China, Jiangxi, 330006, China.

Shu-Ping Jiang (SP)

Key Laboratory of Prevention and Treatment of Cardiovascular and Cerebrovascular Diseases, Ministry of Education, Gannan Medical University, Ganzhou, 341000, China.
School of Basic Medicine, Gannan Medical University, Ganzhou, 341000, China.
Key Laboratory of Biomaterials and Bio-fabrication in Tissue Engineering of Jiangxi Province, Scientific Research Center, Ganzhou, 341000, China.

Jing Li (J)

Department of Pharmacy, National Clinical Research Center for Geriatric Disorders, Xiangya Hospital, Central South University, Changsha, 410008, China.

Zhen Xie (Z)

Key Laboratory of Prevention and Treatment of Cardiovascular and Cerebrovascular Diseases, Ministry of Education, Gannan Medical University, Ganzhou, 341000, China.

Lu-Hua He (LH)

National Engineering Research Center for Modernization of Traditional Chinese Medicine-Hakka Medical Resources Branch, College of Pharmacy, Gannan Medical University, Ganzhou, 341000, China.

Lin Liu (L)

Key Laboratory of Prevention and Treatment of Cardiovascular and Cerebrovascular Diseases, Ministry of Education, Gannan Medical University, Ganzhou, 341000, China.

Yang Liu (Y)

Key Laboratory of Prevention and Treatment of Cardiovascular and Cerebrovascular Diseases, Ministry of Education, Gannan Medical University, Ganzhou, 341000, China.

Classifications MeSH