Paving the way for new and challenging matrix reference materials-particle suspensions at the core of material processing providing RMs for method development and method validation.
Certified reference material
Heterogeneity
Homogeneity
Method validation
Microplastics
Particles
Reference material
Repeatability
Spiking
Suspensions
Journal
Analytical and bioanalytical chemistry
ISSN: 1618-2650
Titre abrégé: Anal Bioanal Chem
Pays: Germany
ID NLM: 101134327
Informations de publication
Date de publication:
Apr 2024
Apr 2024
Historique:
received:
29
09
2023
accepted:
08
11
2023
revised:
03
11
2023
medline:
21
11
2023
pubmed:
21
11
2023
entrez:
21
11
2023
Statut:
ppublish
Résumé
Sufficient homogeneity of the certified parameter(s) over the whole fill series of a matrix reference material (RM) is a fundamental quality criterion. In practice, the heterogeneity of the target parameter is evaluated, whereby a relative value can be calculated of how much the target parameter is varying over the RM-batch. A high degree of homogeneity (low heterogeneity) is an inherent quality mark of a good RM. Here, we report how challenging matrix RMs were produced by using particle suspensions at the core of the material processing step. The examples of matrix RMs produced span from whole water reference materials for persistent organic pollutants, PM
Identifiants
pubmed: 37987767
doi: 10.1007/s00216-023-05046-2
pii: 10.1007/s00216-023-05046-2
doi:
Types de publication
Journal Article
Langues
eng
Sous-ensembles de citation
IM
Pagination
2079-2088Informations de copyright
© 2023. The Author(s).
Références
ISO Guide 30: Reference materials — selected terms and definitions. https://www.iso.org/standard/46209.html . Accessed 18/09/2023.
Seghers J, Stefaniak EA, La Spina R, Cella C, Mehn D, Gilliland D, Held A, Jacobsson U, Emteborg H. Preparation of a reference material for microplastics in water—evaluation of homogeneity. Anal Bioanal Chem. 2022;414:385–97. https://doi.org/10.1007/s00216-021-03198-7 .
doi: 10.1007/s00216-021-03198-7
pubmed: 33547482
Seghers J, Günther M. Breidbach, Peez N, Imhof W, Emteborg H, Feasibility of using quantitative
doi: 10.1007/s00216-023-04567-0
pubmed: 36750474
pmcid: 10284926
van Mourik LM, Crum S, Martinez-Frances E, van Bavel B, Leslie HA, de Boer J, Cofino WP. Results of WEPAL-QUASIMEME/NORMANs first global interlaboratory study on microplastics reveal urgent need for harmonization. Sci Tot Environ. 2021;772: 145071. https://doi.org/10.1016/j.scitotenv.2021.145071 .
doi: 10.1016/j.scitotenv.2021.145071
Charoud-Got J, Emma G, Seghers J, Tumba-Tshilumba MF, Santoro A, Held A, Snell J, Emteborg H. Preparation of a PM2.5-like reference material in sufficient quantities for accurate monitoring of anions and cations in fine atmospheric dust. Anal Bioanal Chem. 2017;409:7121–31. https://doi.org/10.1007/s00216-017-0670-6 .
doi: 10.1007/s00216-017-0670-6
pubmed: 28971237
pmcid: 5717123
Emma G, Snell J, Charoud-Got J, Held A, Emons H. Feasibility study of a candidate reference material for ions in PM2.5: does commutability matter also for inorganic matrices? Anal Bioanal Chem. 2018;410:6001–8. https://doi.org/10.1007/s00216-018-1220-6 .
doi: 10.1007/s00216-018-1220-6
pubmed: 29974149
pmcid: 6096712
European Commission. Directive 2000/60/EC of the European Parliament and of the Council establishing a framework for community action in the field of water policy. European Water Framework Directive (WFD). 2000; https://eur-lex.europa.eu/legal-content/EN/TXT/?uri=CELEX%3A02000L0060-20141120&qid=1695128016959 . Accessed 18/09/2023.
European Commission. Directive 2008/105/EC of the European Parliament and of the Council on environmental quality standards in the field of water policy and amending Directive2000/60/EC. 2008. https://eur-lex.europa.eu/legal-content/EN/TXT/?uri=CELEX%3A02008L0105-20130913&qid=1695128167164 . Accessed 18/09/2023.
European Commission. Directive 2009/90/EC laying down, pursuant to Directive 2000/60/EC of the European Parliament and of the Council, technical specifications for chemical analysis and monitoring of water status. 2009. https://eur-lex.europa.eu/legal-content/EN/TXT/?uri=CELEX%3A32009L0090&qid=1695128664681 . Accessed 18/09/2023.
Elordui-Zapatarietxe S, Fettig I, Philipp R, Gantois F, Lalère B, Swart C, Petrov P, Goenaga-Infante H, Vanermen G, Boom G, Emteborg H. Novel concepts for preparation of reference materials as wholewater samples for priority substances at nanogram-per-liter level using model suspended particulate matter and humic acids. Anal Bioanal Chem. 2015;407:3055–67. https://doi.org/10.1007/s00216-014-8349-8 .
doi: 10.1007/s00216-014-8349-8
pubmed: 25486919
Elordui-Zapatarietxe S, Fettig I, Richter J, Philipp R, Vanermen G, Monteyne E, Boom G, Emteborg H. Preparation and evaluation of sufficiently homogeneous and stable reference materials for priority hazardous substances in whole water. Accred Qual Assur. 2016;21:113–20. https://doi.org/10.1007/s00769-015-1189-1 .
doi: 10.1007/s00769-015-1189-1
Elordui-Zapatarietxe S, Fettig I, Richter J, Philipp R, Gantois F, Lalère B, Swart C, Emteborg H. Interaction of 15 priority substances for water monitoring at ng L
doi: 10.1007/s00769-015-1150-3
Richter J, Elordui-Zapatarietxe S, Emteborg H, Fettig I, Cabillic J, Alasonati E, Gantois F, Swart C, Gokcen T, Tunc M, Binici B, Rodriguez-Cea A, Zuliani T, Gonzalez Gago A, Pröfrock D, Nousiainen M, Sawal G, Buzoianu M, Philipp R. An interlaboratory comparison on whole water samples. Accred Qual Assur. 2016;21:121–9. https://doi.org/10.1007/s00769-015-1190-8 .
doi: 10.1007/s00769-015-1190-8
European Commission, Joint Research Centre, Belz S, Bianchi I, Cella C, Emteborg H, Fumagalli F, Geiss O, Gilliland D, Held A, Jakobsson U, La Spina R, Mehn D, Ramaye Y, Robouch P, Seghers J, Sokull-Kluettgen B, Stefaniak E, Stroka J. Current status of the quantification of microplastics in water : results of a JRC/BAM interlaboratory comparison study on PET in water, Publications Office. 2021. EUR 30799 EN, Publications Office of the European Union, Luxembourg, 2021, ISBN 978–92–76–40958–8. https://data.europa.eu/doi/10.2760/27641 . Accessed 18 Sep 2023.
European Committee for Standardization, CEN. EN 16691: water quality—determination of selected polycyclic aromatic hydrocarbons (PAH) in whole water samples—method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography mass spectrometry (GC–MS). CEN, Brussels, Belgium. 2015.
European Committee for Standardization, CEN. EN 16694: water quality—determination of selected polybrominated diphenyl ether (PBDE) in whole water samples—method using solid phase extraction (SPE) with SPE-disks combined with gas chromatography–mass spectrometry (GC–MS). CEN, Brussels, Belgium. 2015.
European Committee for Standardization, CEN. TS 16692: water quality—determination of tributyltin (TBT) in whole water samples—method using solid phase extraction (SPE) with SPE disks and gas chromatography with triple quadrupole mass spectrometry. CEN, Brussels, Belgium. 2015.
European Commission. Directive 2008/50/EC of the European Parliament and of the Council on ambient air quality and cleaner air for Europe. 2008. https://eur-lex.europa.eu/legal-content/EN/TXT/?uri=CELEX%3A32008L0050&qid=1695128883739 . Accessed 18/09/2023.
CERTIFICATION REPORT, The certification of water-soluble ions in a fine dust (PM
European Committee for Standardization CEN. EN 16913: Ambient air - standard method for measurement of NO
European Committee for Standardisation CEN. European Standard EN 12341:2014. Ambient air - standard gravimetric measurement method for the determination of the PM
CERTIFICATION REPORT The certification of the mass fractions of selected polycyclic aromatic hyrdrocarbons (PAHs) in fine dust (PM
CERTIFICATION REPORT The certification of the mass fractions of arsenic, cadmium, nickel and lead in fine dust (PM
Jenner LC, Rotchell JM, Bennett RT, Cowen M, Tentzeris V, Sadofsky LR. Detection of microplastics in human lung tissue using μFTIR spectroscopy. Sci Total Environ. 2022;831: 154907. https://doi.org/10.1016/j.scitotenv.2022.154907 .
doi: 10.1016/j.scitotenv.2022.154907
pubmed: 35364151
Leslie HA, van Velzen MJM, Brandsma SH, Vethaak AD, Garcia-Vallejo JJ, Lamoree MH. Discovery and quantification of plastic particle pollution in human blood. Environ Int. 2022;163: 107199. https://doi.org/10.1016/j.envint.2022.107199 .
doi: 10.1016/j.envint.2022.107199
pubmed: 35367073
Liu S, Guo J, Liu X, Yang R, Wang H, Sun Y, Chen B, Dong R. Detection of various microplastics in placentas, meconium, infant faeces, breastmilk and infant formula: a pilot prospective study. Sci Total Environ. 2023;854:158699. https://doi.org/10.1016/j.scitotenv.2022.158699 .
doi: 10.1016/j.scitotenv.2022.158699
pubmed: 36108868
Erasmus Maris web page. https://www.erasmusmaris.eu/about-raise-cs.html . Accessed 18/09/2023.
International Organization for Standardization. ISO Guide 35: Reference materials — guidance for characterization and assessment of homogeneity and stability https://www.iso.org/standard/60281.html . Accessed 18 Sep 2023.
CERTIFICATION REPORT The certification of the mass fraction of pesticides in soya: ERM-BC700, EUR 29625 EN, 2019. https://crm.jrc.ec.europa.eu/p/q/erm-bc700+/ERM-BC700-SOYA-BEAN-pesticides/ERM-BC700 . Accessed 18/09/2023.
CERTIFICATION REPORT Certification of the mass fractions of vitamins in whole milk powder: ERM-BD600, EUR 24924 EN, 2011. https://crm.jrc.ec.europa.eu/p/q/vitamins/ERM-BD600-WHOLE-MILK-POWDER-vitamins/ERM-BD600 . Accessed 18/09/2023.
CERTIFICATION REPORT The certification of the mass fractions of elements in pig kidney: ERM-BB186, EUR 25480 EN. 2012. https://crm.jrc.ec.europa.eu/p/q/BB186/ERM-BB186-PIG-KIDNEY-trace-elements/ERM-BB186 . Accessed 18/09/2023.
Wise SA. What if using certified reference materials (CRMs) was a requirement to publish in analytical/bioanalytical chemistry journals? Anal Bioanal Chem. 2022;414:7015–22. https://doi.org/10.1007/s00216-022-04163-8 .
doi: 10.1007/s00216-022-04163-8
pubmed: 35697811
Adams F, Adriaens M. The metamorphosis of analytical chemistry. Anal Bioanal Chem. 2020;412:3525–37. https://doi.org/10.1007/s00216-019-02313-z .
doi: 10.1007/s00216-019-02313-z
pubmed: 31848669
Black G, Lowe C, Anumol T, Bade J, Favela K, Feng Y-L, Knolhoff A, Mceachran A, Nuñez J, Fisher C, Peter K, Soares Quinete N, Sobus J, Sussman E, Watson W, Wickramasekara S, Williams A, Young T. Exploring chemical space in non-targeted analysis: a proposed ChemSpace tool. Anal Bioanal Chem. 2023;415:35–44. https://doi.org/10.1007/s00216-022-04434-4 .
doi: 10.1007/s00216-022-04434-4
pubmed: 36435841
Lehotay SJ. The QuEChERSER Mega-Method. LCGC N Am. 2022;40(1):13–9. https://doi.org/10.56530/lcgc.na.px2173m3 .
doi: 10.56530/lcgc.na.px2173m3
Emteborg H, Florian D, Choquette S, Ellison LR, Fernandes-Whaley M, Mackay L, McCarron P, Panne U, Sander SG, Kim SK, Held A, Linsinger T, Trapmann S. Cooperation in publicly funded reference material production. Accred Qual Assur. 2018;23:371–7. https://doi.org/10.1007/s00769-018-1349-1 .
doi: 10.1007/s00769-018-1349-1
https://www.umweltbundesamt.de/en/topics/chemicals/iesb-specimen-banks/media-center#introducting-to-the-international-environmental-specimen-bank-group . Accessed 18/09/2023.
Roebben G, Rasmussen K, Kestens V, Linsinger TPJ, Rauscher H, Emons H, Stamm H. Reference materials and representative test materials: the nanotechnology case. J Nanopart Res. 2013;15:1455.
doi: 10.1007/s11051-013-1455-2
Wolf W, Andrews KW. A system for defining reference materials applicable to all food matrices. Fresenius J Anal Chem. 1995;352:73–6. https://doi.org/10.1007/BF00322300 .
doi: 10.1007/BF00322300
Sharpless KE, Greenberg RR, Schantz MM, Welch MJ, Wise SA, Ihnat M. Filling the AOAC triangle with food-matrix standard reference materials. Anal Bioanal Chem. 2004;378:1161–7. https://doi.org/10.1007/s00216-003-2384-1 .
doi: 10.1007/s00216-003-2384-1
pubmed: 14689156