ECDD-S16 targets vacuolar ATPase: A potential inhibitor compound for pyroptosis-induced inflammation.


Journal

PloS one
ISSN: 1932-6203
Titre abrégé: PLoS One
Pays: United States
ID NLM: 101285081

Informations de publication

Date de publication:
2023
Historique:
received: 21 06 2023
accepted: 18 09 2023
medline: 29 11 2023
pubmed: 27 11 2023
entrez: 27 11 2023
Statut: epublish

Résumé

Cleistanthin A (CA), extracted from Phyllanthus taxodiifolius Beille, was previously reported as a potential V-ATPase inhibitor relevant to cancer cell survival. In the present study, ECDD-S16, a derivative of cleistanthin A, was investigated and found to interfere with pyroptosis induction via V-ATPase inhibition. This study examined the ability of ECDD-S16 to inhibit endolysosome acidification leading to the attenuation of pyroptosis in Raw264.7 macrophages activated by both surface and endosomal TLR ligands. To elucidate the activity of ECDD-S16 on pyroptosis-induced inflammation, Raw264.7 cells were pretreated with the compound before stimulation with surface and endosomal TLR ligands. The release of lactate dehydrogenase (LDH) was determined by LDH assay. Additionally, the production of cytokines and the expression of pyroptosis markers were examined by ELISA and immunoblotting. Moreover, molecular docking was performed to demonstrate the binding of ECDD-S16 to the vacuolar (V-)ATPase. This study showed that ECDD-S16 could inhibit pyroptosis in Raw264.7 cells activated with surface and endosomal TLR ligands. The attenuation of pyroptosis by ECDD-S16 was due to the impairment of endosome acidification, which also led to decreased Reactive Oxygen Species (ROS) production. Furthermore, molecular docking also showed the possibility of inhibiting endosome acidification by the binding of ECDD-S16 to the vacuolar (V-)ATPase in the region of V0. Our findings indicate the potential of ECDD-S16 for inhibiting pyroptosis and prove that vacuolar H+ ATPase is essential for pyroptosis induced by TLR ligands.

Sections du résumé

BACKGROUND BACKGROUND
Cleistanthin A (CA), extracted from Phyllanthus taxodiifolius Beille, was previously reported as a potential V-ATPase inhibitor relevant to cancer cell survival. In the present study, ECDD-S16, a derivative of cleistanthin A, was investigated and found to interfere with pyroptosis induction via V-ATPase inhibition.
OBJECTIVE OBJECTIVE
This study examined the ability of ECDD-S16 to inhibit endolysosome acidification leading to the attenuation of pyroptosis in Raw264.7 macrophages activated by both surface and endosomal TLR ligands.
METHODS METHODS
To elucidate the activity of ECDD-S16 on pyroptosis-induced inflammation, Raw264.7 cells were pretreated with the compound before stimulation with surface and endosomal TLR ligands. The release of lactate dehydrogenase (LDH) was determined by LDH assay. Additionally, the production of cytokines and the expression of pyroptosis markers were examined by ELISA and immunoblotting. Moreover, molecular docking was performed to demonstrate the binding of ECDD-S16 to the vacuolar (V-)ATPase.
RESULTS RESULTS
This study showed that ECDD-S16 could inhibit pyroptosis in Raw264.7 cells activated with surface and endosomal TLR ligands. The attenuation of pyroptosis by ECDD-S16 was due to the impairment of endosome acidification, which also led to decreased Reactive Oxygen Species (ROS) production. Furthermore, molecular docking also showed the possibility of inhibiting endosome acidification by the binding of ECDD-S16 to the vacuolar (V-)ATPase in the region of V0.
CONCLUSION CONCLUSIONS
Our findings indicate the potential of ECDD-S16 for inhibiting pyroptosis and prove that vacuolar H+ ATPase is essential for pyroptosis induced by TLR ligands.

Identifiants

pubmed: 38011122
doi: 10.1371/journal.pone.0292340
pii: PONE-D-23-19268
pmc: PMC10681236
doi:

Substances chimiques

Vacuolar Proton-Translocating ATPases EC 3.6.1.-
cleistanthin 25047-48-7

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

e0292340

Informations de copyright

Copyright: © 2023 Ekchariyawat et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.

Déclaration de conflit d'intérêts

The authors have declared that no competing interests exist.

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Auteurs

Peeraya Ekchariyawat (P)

Department of Microbiology, Faculty of Public Health, Mahidol University, Bangkok, Thailand.

Rattatammanoon Saengfak (R)

Department of Microbiology, Faculty of Science, Mahidol University, Bangkok, Thailand.

Sucharat Sanongkiet (S)

Department of Chemistry, Faculty of Science, Silpakorn University, Nakhon Pathom, Thailand.

Thanapon Charoenwongpaiboon (T)

Department of Chemistry, Faculty of Science, Silpakorn University, Nakhon Pathom, Thailand.

Suphasuta Khongpraphan (S)

Department of Microbiology, Faculty of Science, Mahidol University, Bangkok, Thailand.

Supaporn Mala (S)

Research Office, Faculty of Dentistry, Mahidol University, Bangkok, Thailand.

Chularat Luangjindarat (C)

Department of Microbiology, Faculty of Science, Mahidol University, Bangkok, Thailand.

Bumrung Munyoo (B)

Excellence Center for Drug Discovery (ECDD), Faculty of Science, Mahidol University, Bangkok, Thailand.

Napason Chabang (N)

School of Bioinnovation and Bio-Based Product Intelligence, Faculty of Science, Mahidol University, Bangkok, Thailand.

Sitthivut Charoensutthivarakul (S)

Excellence Center for Drug Discovery (ECDD), Faculty of Science, Mahidol University, Bangkok, Thailand.
School of Bioinnovation and Bio-Based Product Intelligence, Faculty of Science, Mahidol University, Bangkok, Thailand.
Center for Neuroscience, Faculty of Science, Mahidol University, Bangkok, Thailand.

Suparerk Borwornpinyo (S)

Excellence Center for Drug Discovery (ECDD), Faculty of Science, Mahidol University, Bangkok, Thailand.
Department of Biotechnology, Faculty of Science, Mahidol University, Bangkok, Thailand.

Patoomratana Tuchinda (P)

Excellence Center for Drug Discovery (ECDD), Faculty of Science, Mahidol University, Bangkok, Thailand.

Marisa Ponpuak (M)

Department of Microbiology, Faculty of Science, Mahidol University, Bangkok, Thailand.

Matsayapan Pudla (M)

Department of Oral Microbiology, Faculty of Dentistry, Mahidol University, Bangkok, Thailand.

Pongsak Utaisincharoen (P)

Department of Microbiology, Faculty of Science, Mahidol University, Bangkok, Thailand.

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