Utility of dansyl chloride for the establishment of a sensitive spectrofluorimetric approach for estimating midodrine hydrochloride: application to content uniformity testing.
Journal
RSC advances
ISSN: 2046-2069
Titre abrégé: RSC Adv
Pays: England
ID NLM: 101581657
Informations de publication
Date de publication:
07 Nov 2023
07 Nov 2023
Historique:
received:
14
09
2023
accepted:
01
11
2023
medline:
29
11
2023
pubmed:
29
11
2023
entrez:
29
11
2023
Statut:
epublish
Résumé
A new, straightforward spectrofluorimetric approach with high sensitivity was established for determining midodrine hydrochloride based on derivatizing this drug through its reaction with 5-(dimethylamino)naphthalene-1-sulfonyl chloride (dansyl chloride). The highly fluorescent product was extracted with methylene chloride, and then its emission was measured at 532 nm after excitation at 339 nm. The reaction was conducted in aqueous medium containing 0.1 M borate buffer (pH 8.2). The results showed that the proposed method is sensitive with high linearity in the range from 0.1 to 3 μg mL
Identifiants
pubmed: 38025857
doi: 10.1039/d3ra06268f
pii: d3ra06268f
pmc: PMC10644863
doi:
Types de publication
Journal Article
Langues
eng
Pagination
33453-33458Informations de copyright
This journal is © The Royal Society of Chemistry.
Déclaration de conflit d'intérêts
The authors declare that they have no competing financial interests.
Références
Anesthesiology. 2015 Dec;123(6):1292-300
pubmed: 26492477
J Auton Nerv Syst. 1995 Oct 5;55(1-2):29-35
pubmed: 8690848
Acta Chim Slov. 2013;60(2):256-62
pubmed: 23878928
Luminescence. 2019 Feb;34(1):84-89
pubmed: 30536965
Spectrochim Acta A Mol Biomol Spectrosc. 2022 May 15;273:121046
pubmed: 35240554
JAMA. 1997 Apr 2;277(13):1046-51
pubmed: 9091692
J Chromatogr Sci. 2013 May-Jun;51(5):460-7
pubmed: 23051063
Nephrol Dial Transplant. 2004 Oct;19(10):2553-8
pubmed: 15280522
J Pharm Biomed Anal. 1998 Oct;18(1-2):171-7
pubmed: 9863955
J Chromatogr B Analyt Technol Biomed Life Sci. 2015 Jun 1;991:34-40
pubmed: 25910235
J Pharm Biomed Anal. 2016 Nov 30;131:355-363
pubmed: 27639073
Ann Pharmacother. 2009 Apr;43(4):692-9
pubmed: 19299324
J Pharm Biomed Anal. 2006 Feb 24;40(3):715-9
pubmed: 16242885
J Pharm Biomed Anal. 2023 May 30;229:115322
pubmed: 37001276
Biomed Chromatogr. 1989 Jul;3(4):153-6
pubmed: 2480164
Luminescence. 2019 Dec;34(8):854-858
pubmed: 31338979
Drug Dev Ind Pharm. 2021 Jul;47(7):1072-1078
pubmed: 33818229