Elastocapillarity-driven 2D nano-switches enable zeptoliter-scale liquid encapsulation.


Journal

Nature communications
ISSN: 2041-1723
Titre abrégé: Nat Commun
Pays: England
ID NLM: 101528555

Informations de publication

Date de publication:
02 Jan 2024
Historique:
received: 09 08 2021
accepted: 03 12 2023
medline: 4 1 2024
pubmed: 4 1 2024
entrez: 3 1 2024
Statut: epublish

Résumé

Biological nanostructures change their shape and function in response to external stimuli, and significant efforts have been made to design artificial biomimicking devices operating on similar principles. In this work we demonstrate a programmable nanofluidic switch, driven by elastocapillarity, and based on nanochannels built from layered two-dimensional nanomaterials possessing atomically smooth surfaces and exceptional mechanical properties. We explore operational modes of the nanoswitch and develop a theoretical framework to explain the phenomenon. By predicting the switching-reversibility phase diagram-based on material, interfacial and wetting properties, as well as the geometry of the nanofluidic circuit-we rationally design switchable nano-capsules capable of enclosing zeptoliter volumes of liquid, as small as the volumes enclosed in viruses. The nanoswitch will find useful application as an active element in integrated nanofluidic circuitry and could be used to explore nanoconfined chemistry and biochemistry, or be incorporated into shape-programmable materials.

Identifiants

pubmed: 38167702
doi: 10.1038/s41467-023-44200-3
pii: 10.1038/s41467-023-44200-3
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

185

Subventions

Organisme : Lloyd's Register Foundation (LRF)
ID : Designer Nanomaterials
Organisme : Lloyd's Register Foundation (LRF)
ID : Designer Nanomaterials
Organisme : National Research Foundation Singapore (National Research Foundation-Prime Minister's office, Republic of Singapore)
ID : NRF-CRP13-2014-03
Organisme : Ministry of Education - Singapore (MOE)
ID : MOE-T2EP50221-0018

Informations de copyright

© 2024. The Author(s).

Références

Coste, B. et al. Piezo proteins are pore-forming subunits of mechanically activated channels. Nature 483, 176–181 (2012).
pubmed: 22343900 pmcid: 3297710 doi: 10.1038/nature10812
McEvoy, M. A. & Correll, N. Materials that couple sensing, actuation, computation, and communication. Science 347, 1261689 (2015).
Bocquet, L. Nanofluidics coming of age. Nat. Mater. 19, 254–256 (2020).
pubmed: 32099111 doi: 10.1038/s41563-020-0625-8
Geim, A. K. Exploring two-dimensional empty space. Nano Lett. 21, 6356–6358 (2021).
pubmed: 34296884 doi: 10.1021/acs.nanolett.1c02591
Blees, M. K. et al. Graphene kirigami. Nature 524, 204–207 (2015).
pubmed: 26222025 doi: 10.1038/nature14588
Miskin, M. Z. et al. Graphene-based bimorphs for micron-sized, tautonomous origami machines. Proc. Natl. Acad. Sci. USA 115, 466–470 (2018).
pubmed: 29295917 pmcid: 5776973 doi: 10.1073/pnas.1712889115
Reynolds, M. F. et al. Capillary origami with atomically thin membranes. Nano Lett. 19, 6221–6226 (2019).
pubmed: 31430164 doi: 10.1021/acs.nanolett.9b02281
Acome, E. et al. Hydraulically amplified self-healing electrostatic actuators with muscle-like performance. Science 359, 61–65 (2018).
pubmed: 29302008 doi: 10.1126/science.aao6139
Miskin, M. Z. et al. Electronically integrated, mass-manufactured, microscopic robots. Nature 584, 557–561 (2020).
pubmed: 32848225 doi: 10.1038/s41586-020-2626-9
Fan, X., Chung, J. Y., Lim, Y. X., Li, Z. & Loh, X. J. Review of adaptive programmable materials and their bioapplications. ACS Appl. Mater. Interfaces 8, 33351–33370 (2016).
pubmed: 27960431 doi: 10.1021/acsami.6b09110
Thorsen, T., Maerkl, S. J. & Quake, S. R. Microfluidic large-scale integration. Science 298, 580–584 (2002).
pubmed: 12351675 doi: 10.1126/science.1076996
Xu, Y., Shinomiya, M. & Harada, A. Soft matter-regulated active nanovalves locally self-assembled in femtoliter nanofluidic channels. Adv. Mater. 28, 2209–2216 (2016).
pubmed: 26786725 doi: 10.1002/adma.201505132
Sano, H., Kazoe, Y., Morikawa, K. & Kitamori, T. Implementation of a nanochannel open/close valve into a glass nanofluidic device. Microfluid Nanofluid 24, 78 (2020).
doi: 10.1007/s10404-020-02383-x
de Gennes, P.-G., Brochard-Wyart, F. & Quéré, D. Capillarity and Wetting Phenomena (Springer, 2004).
Stroock, A. D., Pagay, V. V., Zwieniecki, M. A. & Michele Holbrook, N. The physicochemical hydrodynamics of vascular plants. Annu. Rev. Fluid Mech. 46, 615–642 (2014).
doi: 10.1146/annurev-fluid-010313-141411
Van Honschoten, J. W., Brunets, N. & Tas, N. R. Capillarity at the nanoscale. Chem. Soc. Rev. 39, 1096–1114 (2010).
pubmed: 20179827 doi: 10.1039/b909101g
Style, R. W., Jagota, A., Hui, C.-Y. & Dufresne, E. R. Elastocapillarity: surface tension and the mechanics of soft solids. Annu. Rev. Condens. Matter Phys. 8, 99–118 (2017).
doi: 10.1146/annurev-conmatphys-031016-025326
Bico, J., Reyssat, É. & Roman, B. Elastocapillarity: when surface tension deforms elastic solids. Annu. Rev. Fluid Mech. 50, 629–659 (2018).
doi: 10.1146/annurev-fluid-122316-050130
Mastrangelo, C. H. & Hsu, C. H. Mechanical stability and adhesion of microstructures under capillary forces. II. Experiments. J. Microelectromechan. Syst. 2, 44–55 (1993).
doi: 10.1109/84.232594
Tas, N., Sonnenberg, T., Jansen, H., Legtenberg, R. & Elwenspoek, M. Stiction in surface micromachining. J. Micromech. Microeng. 6, 385–397 (1996).
doi: 10.1088/0960-1317/6/4/005
Geim, A. K. & Grigorieva, I. V. Van der Waals heterostructures. Nature 499, 419–425 (2013).
pubmed: 23887427 doi: 10.1038/nature12385
Radha, B. et al. Molecular transport through capillaries made with atomic-scale precision. Nature 538, 222–225 (2016).
pubmed: 27602512 doi: 10.1038/nature19363
Esfandiar, A. et al. Size effect in ion transport through angstrom-scale slits. Science 358, 511–513 (2017).
pubmed: 29074772 doi: 10.1126/science.aan5275
Fumagalli, L. et al. Anomalously low dielectric constant of confined water. Science 360, 1339–1342 (2018).
pubmed: 29930134 doi: 10.1126/science.aat4191
Yang, Q. et al. Capillary condensation under atomic-scale confinement. Nature 588, 250–253 (2020).
pubmed: 33299189 doi: 10.1038/s41586-020-2978-1
Abendroth, J. M., Bushuyev, O. S., Weiss, P. S. & Barrett, C. J. Controlling motion at the nanoscale: rise of the molecular machines. ACS Nano 9, 7746–7768 (2015).
pubmed: 26172380 doi: 10.1021/acsnano.5b03367
Ekinci, K. L. Electromechanical transducers at the nanoscale: actuation and sensing of motion in nanoelectromechanical systems (NEMS). Small 1, 786–797 (2005).
pubmed: 17193524 doi: 10.1002/smll.200500077
Tas, N. R., Escalante, M., Van Honschoten, J. W., Jansen, H. V. & Elwenspoek, M. Capillary negative pressure measured by nanochannel collapse. Langmuir 26, 1473–1476 (2010).
pubmed: 20047328 doi: 10.1021/la903649n
Kang, S. H., Pokroy, B., Mahadevan, L. & Aizenberg, J. Control of shape and size of nanopillar assembly by adhesion-mediated elastocapillary interaction. ACS Nano 4, 6323–6331 (2010).
pubmed: 21038896 doi: 10.1021/nn102260t
Vrancken, N. et al. Nanoscale elastocapillary effect induced by thin-liquid-film instability. J. Phys. Chem. Lett. 11, 2751–2758 (2020).
pubmed: 32187494 doi: 10.1021/acs.jpclett.0c00218
Van Honschoten, J. W., Escalante, M., Tas, N. R., Jansen, H. V. & Elwenspoek, M. Elastocapillary filling of deformable nanochannels. J. Appl. Phys. 101, 094310 (2007).
Park, J.-G. et al. Interfacial and electrokinetic characterization of IPA solutions related to semiconductor wafer drying and cleaning. J. Electrochem. Soc. 153, G811 (2006).
doi: 10.1149/1.2214532
Bunch, J. S. et al. Impermeable atomic membranes from graphene sheets. Nano Lett. 8, 2458–2462 (2008).
pubmed: 18630972 doi: 10.1021/nl801457b
Wang, G. et al. Bending of multilayer van der Waals materials. Phys. Rev. Lett. 123, 116101 (2019).
pubmed: 31573244 doi: 10.1103/PhysRevLett.123.116101
Anoop, R. & Sen, A. K. Capillary flow enhancement in rectangular polymer microchannels with a deformable wall. Phys. Rev. E 92, 013024 (2015).
doi: 10.1103/PhysRevE.92.013024
Kozbial, A., Trouba, C., Liu, H. & Li, L. Characterization of the intrinsic water wettability of graphite using contact angle measurements: effect of defects on static and dynamic contact angles. Langmuir 33, 959–967 (2017).
pubmed: 28071919 doi: 10.1021/acs.langmuir.6b04193
Williams, R. & Goodman, A. M. Wetting of thin layers of SiO
doi: 10.1063/1.1655297
Cheng, S. & Robbins, M. O. Nanocapillary adhesion between parallel plates. Langmuir 32, 7788–7795 (2016).
pubmed: 27413872 doi: 10.1021/acs.langmuir.6b02024
Koenig, S. P., Boddeti, N. G., Dunn, M. L. & Bunch, J. S. Ultrastrong adhesion of graphene membranes. Nat. Nanotech 6, 543–546 (2011).
doi: 10.1038/nnano.2011.123
Boddeti, N. G. et al. Mechanics of adhered, pressurized graphene blisters. J. Appl. Mechan. 80, 040909 (2013).
Han, E. et al. Ultrasoft slip-mediated bending in few-layer graphene. Nat. Mater. 19, 305–309 (2020).
pubmed: 31712745 doi: 10.1038/s41563-019-0529-7
Khestanova, E., Guinea, F., Fumagalli, L., Geim, A. K. & Grigorieva, I. V. Universal shape and pressure inside bubbles appearing in van der Waals heterostructures. Nat. Commun. 7, 1–10 (2016).
doi: 10.1038/ncomms12587
Sanchez, D. A. et al. Mechanics of spontaneously formed nanoblisters trapped by transferred 2D crystals. Proc. Natl. Acad. Sci. USA 115, 7884–7889 (2018).
pubmed: 30006468 pmcid: 6077740 doi: 10.1073/pnas.1801551115
Sanchez, D. A., Dai, Z. & Lu, N. 2D material bubbles: fabrication, characterization, and applications. Trends Chem. 3, 204–217 (2021).
doi: 10.1016/j.trechm.2020.12.011
Megra, Y. T. & Suk, J. W. Adhesion properties of 2D materials. J. Phys. D Appl. Phys. 52, 364002 (2019).
doi: 10.1088/1361-6463/ab27ad
Dai, Z., Lu, N., Liechti, K. M. & Huang, R. Mechanics at the interfaces of 2D materials: challenges and opportunities. Curr. Opin. Solid State Mater. Sci. 24, 100837 (2020).
doi: 10.1016/j.cossms.2020.100837
Gopinadhan, K. et al. Complete steric exclusion of ions and proton transport through confined monolayer water. Science 363, 145–148 (2019).
pubmed: 30630924 doi: 10.1126/science.aau6771
Vogel, M. J. & Steen, P. H. Capillarity-based switchable adhesion. Proc. Natl. Acad. Sci. USA 107, 3377–3381 (2010).
pubmed: 20133725 pmcid: 2840443 doi: 10.1073/pnas.0914720107
Grommet, A. B., Feller, M. & Klajn, R. Chemical reactivity under nanoconfinement. Nat. Nanotechnol. 15, 256–271 (2020).
pubmed: 32303705 doi: 10.1038/s41565-020-0652-2

Auteurs

Nathan Ronceray (N)

Department of Physics, National University of Singapore, Singapore, 117551, Singapore.
Centre for Advanced 2D Materials, National University of Singapore, Singapore, 117542, Singapore.

Massimo Spina (M)

Department of Physics, National University of Singapore, Singapore, 117551, Singapore.
Centre for Advanced 2D Materials, National University of Singapore, Singapore, 117542, Singapore.

Vanessa Hui Yin Chou (VHY)

Centre for Advanced 2D Materials, National University of Singapore, Singapore, 117542, Singapore.

Chwee Teck Lim (CT)

Department of Biomedical Engineering, National University of Singapore, Singapore, 117583, Singapore.
Institute for Health Innovation and Technology (iHealthtech), National University of Singapore, Singapore, 119276, Singapore.
Mechanobiology Institute, National University of Singapore, Singapore, 117411, Singapore.

Andre K Geim (AK)

National Graphene Institute, University of Manchester, Manchester, M13 9PL, UK.

Slaven Garaj (S)

Department of Physics, National University of Singapore, Singapore, 117551, Singapore. slaven@nus.edu.sg.
Centre for Advanced 2D Materials, National University of Singapore, Singapore, 117542, Singapore. slaven@nus.edu.sg.
Department of Biomedical Engineering, National University of Singapore, Singapore, 117583, Singapore. slaven@nus.edu.sg.
Department of Material Science Engineering, National University of Singapore, Singapore, 117575, Singapore. slaven@nus.edu.sg.

Classifications MeSH