Reaction of Picolinamides with Ketones Producing a New Type of Heterocyclic Salts with an Imidazolidin-4-One Ring.

NMR and FT-IR spectroscopy X-ray study imidazolidin-4-ones quantum-chemical calculations sulfobetaines

Journal

Molecules (Basel, Switzerland)
ISSN: 1420-3049
Titre abrégé: Molecules
Pays: Switzerland
ID NLM: 100964009

Informations de publication

Date de publication:
29 Dec 2023
Historique:
received: 02 11 2023
revised: 20 12 2023
accepted: 22 12 2023
medline: 11 1 2024
pubmed: 11 1 2024
entrez: 11 1 2024
Statut: epublish

Résumé

Reactions of picolinamides with 1,3-propanesultone in methanol followed by the treatment with ketones led to a series of previously unknown chemical transformations, yielding first pyridinium salts (

Identifiants

DOI: 10.3390/molecules29010206 PMID: 38202789
pubmed: 38202789
pii: molecules29010206
doi: 10.3390/molecules29010206
pii:
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Subventions

Organisme : Russian Science Foundation
ID : 21-73-20250

Auteurs

Eugenia P Kramarova (EP)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.

Dmitry N Lyakhmun (DN)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.

Dmitry V Tarasenko (DV)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.

Sophia S Borisevich (SS)

Ufa Institute of Chemistry, Oktyabrya Aven., 71, 450054 Ufa, Russia.

Edward M Khamitov (EM)

Ufa Institute of Chemistry, Oktyabrya Aven., 71, 450054 Ufa, Russia.
ORCID: 0000-0001-8987-4254

Alfia R Yusupova (AR)

Ufa Institute of Chemistry, Oktyabrya Aven., 71, 450054 Ufa, Russia.

Alexander A Korlyukov (AA)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.
A.N.Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Vavilova St. 28, Bl. 1, 119334 Moscow, Russia.
ORCID: 0000-0002-5600-9886

Alexander R Romanenko (AR)

A.N.Nesmeyanov Institute of Organoelement Compounds of Russian Academy of Sciences, Vavilova St. 28, Bl. 1, 119334 Moscow, Russia.
D.I. Mendeleev Russian University of Chemical Technology, Miusskaya Sq., 9, 125047 Moscow, Russia.

Tatiana A Shmigol (TA)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.

Sergey Yu Bylikin (SY)

The Open University, Walton Hall, Milton Keynes MK7 6BJ, UK.

Yuri I Baukov (YI)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.

Vadim V Negrebetsky (VV)

Institute of Pharmacy and Medical Chemistry, Pirogov Russian National Research Medical University, Ostrovityanov St., Bl. 1, 117997 Moscow, Russia.
ORCID: 0000-0001-6852-8942

Classifications MeSH