Fractionation of High-Value Compounds from Hops Using an Optimised Sequential Extraction Procedure.

antioxidant activity hop bitter acids hops phenolic compounds sequential extraction xanthohumol

Journal

Antioxidants (Basel, Switzerland)
ISSN: 2076-3921
Titre abrégé: Antioxidants (Basel)
Pays: Switzerland
ID NLM: 101668981

Informations de publication

Date de publication:
26 Dec 2023
Historique:
received: 13 11 2023
revised: 11 12 2023
accepted: 20 12 2023
medline: 22 1 2024
pubmed: 22 1 2024
entrez: 22 1 2024
Statut: epublish

Résumé

This study describes the development and optimisation of a process for the extraction and fractionation of high-value compounds from hops. Firstly, the efficacy of ten organic solvents was compared for performing the initial solid-liquid extraction of compounds from hop pellets with subsequent fractionation steps. A methanol-dichloromethane mixture was selected and the extraction variables were optimised in order to maximise the recovery of valuable hop compounds separated into different streams (α- and β-acids in soft resins, xanthohumol in hard resins, and phenolics in spent solids) after fractionation steps. The optimisation results showed that extraction of hop pellets performed at room temperature with 19.7% (

Identifiants

pubmed: 38247470
pii: antiox13010045
doi: 10.3390/antiox13010045
pii:
doi:

Types de publication

Journal Article

Langues

eng

Subventions

Organisme : European Union's Horizon 2020 Research and Innovation Programe
ID : LIGNICOAT project Grant number: 101023342
Organisme : European Agricultural Funds for Rural Development (FEADER funds)
ID : AGRORECOVERY

Déclaration de conflit d'intérêts

The authors declare no conflicts of interest.

Auteurs

Ana I Paniagua-García (AI)

Centre of Biofuels and Bioproducts, Agricultural Technological Institute of Castilla y León, Villarejo de Órbigo, E-24358 León, Spain.

David Ruano-Rosa (D)

Agricultural Technological Institute of Castilla y León, Ctra. De Burgos, Km 119, E-47071 Valladolid, Spain.

Rebeca Díez-Antolínez (R)

Centre of Biofuels and Bioproducts, Agricultural Technological Institute of Castilla y León, Villarejo de Órbigo, E-24358 León, Spain.

Classifications MeSH