Development and validation of a classification model for boar taint detection in pork fat samples.

Boar taint Foodomics GC×GC-TOFMS Statistical analysis UHPLC-MS/MS Untargeted volatolomics

Journal

Food chemistry
ISSN: 1873-7072
Titre abrégé: Food Chem
Pays: England
ID NLM: 7702639

Informations de publication

Date de publication:
26 Jan 2024
Historique:
received: 06 10 2023
revised: 22 01 2024
accepted: 23 01 2024
medline: 1 2 2024
pubmed: 1 2 2024
entrez: 31 1 2024
Statut: aheadofprint

Résumé

This study aims to characterize a complete volatile organic compound profile of pork neck fat for boar taint prediction. The objectives are to identify specific compounds related to boar taint and to develop a classification model. In addition to the well-known androstenone, skatole and indole, 10 other features were found to be discriminant according to untargeted volatolomic analyses were conducted on 129 samples using HS-SPME-GC×GC-TOFMS. To select the odor-positive samples among the 129 analyzed, the selection was made by combining human nose evaluations with the skatole and androstenone concentrations determined using UHPLC-MS/MS. A comparison of the data of the two populations was performed and a statistical model analysis was built on 70 samples out of the total of 129 samples fully positive or fully negative through these two orthogonal methods for tainted prediction. Then, the model was applied to the 59 remaining samples. Finally, 7 samples were classified as tainted.

Identifiants

pubmed: 38295570
pii: S0308-8146(24)00220-6
doi: 10.1016/j.foodchem.2024.138572
pii:
doi:

Types de publication

Journal Article

Langues

eng

Sous-ensembles de citation

IM

Pagination

138572

Informations de copyright

Copyright © 2024 Elsevier Ltd. All rights reserved.

Déclaration de conflit d'intérêts

Declaration of competing interest The authors declare that they have no known competing financial interests or personal relationships that could have appeared to influence the work reported in this paper.

Auteurs

Anaïs Rodrigues (A)

Organic and Biological Analytical Chemistry Group, MolSys Research Unit, University of Liège, 4000 Liège, Belgium. Electronic address: anais.rodrigues@uliege.be.

Thibault Massenet (T)

Organic and Biological Analytical Chemistry Group, MolSys Research Unit, University of Liège, 4000 Liège, Belgium. Electronic address: thibault.massenet@uliege.be.

Lena M Dubois (LM)

Organic and Biological Analytical Chemistry Group, MolSys Research Unit, University of Liège, 4000 Liège, Belgium. Electronic address: lena_dubois@leco.com.

Anne-Catherine Huet (AC)

CER Groupe, Analytical Laboratory, 6900 Marloie, Belgium. Electronic address: ac.huet@cergroupe.be.

Alice Markey (A)

TERRA Teaching and Research Center, Gembloux Agro-Bio Tech, University of Liège, 5030 Gembloux, Belgium. Electronic address: alice.markey@uliege.be.

José Wavreille (J)

Animal Production Unit, Walloon Agricultural Research Centre, 5030 Gembloux, Belgium. Electronic address: j.wavreille@cra.wallonie.be.

Nicolas Gengler (N)

TERRA Teaching and Research Center, Gembloux Agro-Bio Tech, University of Liège, 5030 Gembloux, Belgium. Electronic address: nicolas.gengler@uliege.be.

Pierre-Hugues Stefanuto (PH)

Organic and Biological Analytical Chemistry Group, MolSys Research Unit, University of Liège, 4000 Liège, Belgium. Electronic address: phstefanuto@uliege.be.

Jean-François Focant (JF)

Organic and Biological Analytical Chemistry Group, MolSys Research Unit, University of Liège, 4000 Liège, Belgium. Electronic address: jf.focant@uliege.be.

Classifications MeSH